1-phenyl-r-1,c-2,c-3-trideuteriocyclopropane

Base Information

Chemical Name:1-phenyl-r-1,c-2,c-3-trideuteriocyclopropane
CAS No.:88546-75-2
Molecular Formula:C₉H₁₀
Molecular Weight:121.155
Hs Code.:

Synonyms:1-phenyl-r-1,c-2,c-3-trideuteriocyclopropane

Suppliers and Price of 1-phenyl-r-1,c-2,c-3-trideuteriocyclopropane

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 1-phenyl-r-1,c-2,c-3-trideuteriocyclopropane

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 1-phenyl-r-1,c-2,c-3-trideuteriocyclopropane

There total 7 articles about 1-phenyl-r-1,c-2,c-3-trideuteriocyclopropane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

: c-2-phenyl-1,2,t-3-trideuteriocyclopropanecarbaldehyde

: 88546-75-2
1-phenyl-r-1,c-2,c-3-trideuteriocyclopropane

Guidance literature:: With Wilkinson's catalyst; In benzene; for 17h; Heating;
DOI:10.1021/ja00317a038

Reference yield:

: 52751-11-8
cis<α,β-2H2>styrene

: 88546-75-2
1-phenyl-r-1,c-2,c-3-trideuteriocyclopropane

Guidance literature:: Multi-step reaction with 6 steps

1: 63 percent / chiral copper(II) catalyst / cyclohexane / 67 °C

2: 25 percent aq. NaOH / methanol / 12.5 h / Heating

4: 100 percent / LiAlH₄ / diethyl ether / 2.5 h / Heating

5: 100 percent / pyridinium chlorochromate

6: 69 percent / chlorotris(triphenylphosphine)rhodium(I) / benzene / 17 h / Heating

With sodium hydroxide; Wilkinson's catalyst; lithium aluminium tetrahydride; pyridinium chlorochromate; chiral copper(II) catalyst; In methanol; diethyl ether; cyclohexane; benzene;
DOI:10.1021/ja00317a038

Reference yield:

: (dl)-menthyl 2-phenyltrideuteriocyclopropanecarboxylate

: 88546-75-2
1-phenyl-r-1,c-2,c-3-trideuteriocyclopropane

Guidance literature:: Multi-step reaction with 5 steps

1: 25 percent aq. NaOH / methanol / 12.5 h / Heating

3: 100 percent / LiAlH₄ / diethyl ether / 2.5 h / Heating

4: 100 percent / pyridinium chlorochromate

5: 69 percent / chlorotris(triphenylphosphine)rhodium(I) / benzene / 17 h / Heating

With sodium hydroxide; Wilkinson's catalyst; lithium aluminium tetrahydride; pyridinium chlorochromate; In methanol; diethyl ether; benzene;
DOI:10.1021/ja00317a038