FeBr(C₅H₂N)4(C₆H₄CH₃)3(C₆H₄NCS)

Base Information

• Chemical Name: FeBr(C₅H₂N)4(C₆H₄CH₃)3(C₆H₄NCS)
• CAS No.: 198336-61-7
• Molecular Formula: C₄₈H₃₃BrFeN₅S
• Molecular Weight: 847.641
• Mol file: 198336-61-7.mol

Synonyms:FeBr(C₅H₂N)4(C₆H₄CH₃)3(C₆H₄NCS)

Chemical Property of FeBr(C₅H₂N)4(C₆H₄CH₃)3(C₆H₄NCS)

Chemical Property:

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Technology Process of FeBr(C₅H₂N)4(C₆H₄CH₃)3(C₆H₄NCS)

There total 1 articles about FeBr(C₅H₂N)4(C₆H₄CH₃)3(C₆H₄NCS) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

(C5H2N)4(C6H4CH3)3(C6H4NCS)H2 + iron(II) bromide (7789-46-0) → FeBr(C5H2N)4(C6H4CH3)3(C6H4NCS) (198336-61-7)

Guidance literature:

With air; In dichloromethane; chloroform; acetonitrile; Fe-salt dissoln. in refluxing CH3CN over several min, cooling to 50°C, org. compd. soln. in N2-purged CHCl3 addn. , mixt. stirring for 15min (N2), exposition to air, diln. (CH2Cl2), stirring with satd. NaCl s oln. in 1 M HCl; org. phase washing (water), sepn. from water phase, solvent vac. evapn.,flash chromy. (silica gel, CH2Cl2/MeOH);

DOI:10.1021/jp972510u

upstream raw materials:

iron(II) bromide