l-8-phenylmenthyl endo-5-methyl-4,6-dioxo-3-oxa-5-azatricyclo<6.2.1.0^2,7>undec-9-ene-7-carboxylate

Base Information

• Chemical Name: l-8-phenylmenthyl endo-5-methyl-4,6-dioxo-3-oxa-5-azatricyclo<6.2.1.0^2,7>undec-9-ene-7-carboxylate
• CAS No.: 124595-65-9
• Molecular Formula: C₂₇H₃₃NO₅
• Molecular Weight: 451.563

Synonyms:l-8-phenylmenthyl endo-5-methyl-4,6-dioxo-3-oxa-5-azatricyclo<6.2.1.0^2,7>undec-9-ene-7-carboxylate

Chemical Property of l-8-phenylmenthyl endo-5-methyl-4,6-dioxo-3-oxa-5-azatricyclo<6.2.1.0^2,7>undec-9-ene-7-carboxylate

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Technology Process of l-8-phenylmenthyl endo-5-methyl-4,6-dioxo-3-oxa-5-azatricyclo<6.2.1.0^2,7>undec-9-ene-7-carboxylate

There total 3 articles about l-8-phenylmenthyl endo-5-methyl-4,6-dioxo-3-oxa-5-azatricyclo<6.2.1.0^2,7>undec-9-ene-7-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 53.0%

cyclopenta-1,3-diene (542-92-7,25568-84-7,7313-32-8) + l-8-phenylmenthyl 2,4-dioxo-3-methyl-1,3-oxazine-5-carboxylate (124595-62-6) → l-8-phenylmenthyl endo-5-methyl-4,6-dioxo-3-oxa-5-azatricyclo<6.2.1.02,7>undec-9-ene-7-carboxylate (124595-65-9)

Guidance literature:

titanium tetrachloride; In dichloromethane; at -78 ℃; for 1h;

DOI:10.1248/cpb.37.933

Reference yield: 43.4%

cyclopenta-1,3-diene (542-92-7,25568-84-7,7313-32-8) + l-8-phenylmenthyl 2,4-dioxo-3-methyl-1,3-oxazine-5-carboxylate (124595-62-6) → l-8-phenylmenthyl endo- and exo-5-methyl-4,6-dioxo-3-oxa-5-azatricyclo<6.2.1.02,7>undec-9-ene-7-carboxylate (124595-65-9,124648-99-3)

Guidance literature:

In dichloromethane; for 48h; Ambient temperature;

DOI:10.1248/cpb.37.933

Reference yield:

cyclopenta-1,3-diene (542-92-7,25568-84-7,7313-32-8) + l-8-phenylmenthyl 2,4-dioxo-3-methyl-1,3-oxazine-5-carboxylate (124595-62-6) → l-8-phenylmenthyl endo-5-methyl-4,6-dioxo-3-oxa-5-azatricyclo<6.2.1.02,7>undec-9-ene-7-carboxylate (124595-65-9) + l-8-phenylmenthyl-exo-5-methyl-4,6-dioxo-3-oxa-5-azatricyclo<6.2.1.02,7>undec-9-ene-7-carboxylate (124648-99-3)

Guidance literature:

In dichloromethane; for 48h; Yield given. Yields of byproduct given. Title compound not separated from byproducts; Ambient temperature;

DOI:10.1248/cpb.37.933

upstream raw materials:

cyclopenta-1,3-diene

l-8-phenylmenthyl 2,4-dioxo-3-methyl-1,3-oxazine-5-carboxylate

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