octyl (2,3,4-tri-O-acetyl-β-D-fucopyranosyl)-(1->4)-(3,6-di-O-benzyl-2-deoxy-2-phthalimido-β-D-glucopyranosyl)-(1->2)-3,4,6-tri-O-benzyl-α-D-mannopyranoside

Base Information

• Chemical Name: octyl (2,3,4-tri-O-acetyl-β-D-fucopyranosyl)-(1->4)-(3,6-di-O-benzyl-2-deoxy-2-phthalimido-β-D-glucopyranosyl)-(1->2)-3,4,6-tri-O-benzyl-α-D-mannopyranoside
• CAS No.: 629620-17-3
• Molecular Formula: C₇₅H₈₇NO₁₉
• Molecular Weight: 1306.51

Synonyms:octyl (2,3,4-tri-O-acetyl-β-D-fucopyranosyl)-(1->4)-(3,6-di-O-benzyl-2-deoxy-2-phthalimido-β-D-glucopyranosyl)-(1->2)-3,4,6-tri-O-benzyl-α-D-mannopyranoside

Chemical Property of octyl (2,3,4-tri-O-acetyl-β-D-fucopyranosyl)-(1->4)-(3,6-di-O-benzyl-2-deoxy-2-phthalimido-β-D-glucopyranosyl)-(1->2)-3,4,6-tri-O-benzyl-α-D-mannopyranoside

Chemical Property:

Purity/Quality:

98% ^*data from raw suppliers

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Technology Process of octyl (2,3,4-tri-O-acetyl-β-D-fucopyranosyl)-(1->4)-(3,6-di-O-benzyl-2-deoxy-2-phthalimido-β-D-glucopyranosyl)-(1->2)-3,4,6-tri-O-benzyl-α-D-mannopyranoside

There total 1 articles about octyl (2,3,4-tri-O-acetyl-β-D-fucopyranosyl)-(1->4)-(3,6-di-O-benzyl-2-deoxy-2-phthalimido-β-D-glucopyranosyl)-(1->2)-3,4,6-tri-O-benzyl-α-D-mannopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

ethyl 2,3,4-tri-O-acetyl-6-deoxy-1-thio-β-D-galactopyranoside (160533-93-7) + octyl (3,6-di-O-benzyl-2-deoxy-2-phthalimido-β-D-glucopyranosyl)-(1->2)-3,4,6-tri-O-benzyl-α-D-mannopyranoside → octyl (2,3,4-tri-O-acetyl-β-D-fucopyranosyl)-(1->4)-(3,6-di-O-benzyl-2-deoxy-2-phthalimido-β-D-glucopyranosyl)-(1->2)-3,4,6-tri-O-benzyl-α-D-mannopyranoside (629620-17-3)

Guidance literature:

With bromine; silver trifluoromethanesulfonate; In dichloromethane; toluene;

DOI:10.1002/ejoc.200300293

Reference yield:

octyl (2,3,4-tri-O-acetyl-β-D-fucopyranosyl)-(1->4)-(3,6-di-O-benzyl-2-deoxy-2-phthalimido-β-D-glucopyranosyl)-(1->2)-3,4,6-tri-O-benzyl-α-D-mannopyranoside (629620-17-3) → (2S,3R,4S,5R,6R)-2-[(2R,3S,4R,5R,6S)-5-Amino-4-benzyloxy-2-benzyloxymethyl-6-((2S,3S,4S,5R,6R)-4,5-bis-benzyloxy-6-benzyloxymethyl-2-octyloxy-tetrahydro-pyran-3-yloxy)-tetrahydro-pyran-3-yloxy]-6-methyl-tetrahydro-pyran-3,4,5-triol

Guidance literature:

With ethylenediamine; In butan-1-ol; at 90 ℃;

DOI:10.1002/ejoc.200300293

upstream raw materials:

ethyl 2,3,4-tri-O-acetyl-6-deoxy-1-thio-β-D-galactopyranoside

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