3-(benzyloxy)propyl trifluoromethanesulfonate

Base Information

Chemical Name:3-(benzyloxy)propyl trifluoromethanesulfonate
CAS No.:154732-05-5
Molecular Formula:C₁₁H₁₃F₃O₄S
Molecular Weight:298.283
Hs Code.:

Synonyms:3-(benzyloxy)propyl trifluoromethanesulfonate

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Chemical Property of 3-(benzyloxy)propyl trifluoromethanesulfonate

Chemical Property:

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Technology Process of 3-(benzyloxy)propyl trifluoromethanesulfonate

There total 2 articles about 3-(benzyloxy)propyl trifluoromethanesulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 358-23-6
trifluoromethylsulfonic anhydride

: 4799-68-2
3-benzyloxypropan-1-ol

: 154732-05-5
3-(benzyloxy)propyl trifluoromethanesulfonate

Guidance literature:: With triethylamine; In dichloromethane; at 0 ℃; for 1.5h; Inert atmosphere;
DOI:10.1021/ol202629d

Reference yield:

: 100-44-7
benzyl chloride

: 154732-05-5
3-(benzyloxy)propyl trifluoromethanesulfonate

Guidance literature:: Multi-step reaction with 2 steps

1: NaOH / dimethylformamide

2: 2,6-lutidine / CH₂Cl₂

With 2,6-dimethylpyridine; sodium hydroxide; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/S0040-4039(98)01841-3

Reference yield: 81.0%

: 56596-18-0
4-allyldihydrofuran-2(3H)-one

: 154732-05-5
3-(benzyloxy)propyl trifluoromethanesulfonate

: rel-(3S,4S)-4-allyl-3-(3-benzyloxypropyl)dihydrofuran-2(3H)-one

Guidance literature:: 4-allyldihydrofuran-2(3H)-one; With potassium hexamethylsilazane; In tetrahydrofuran; toluene; at -78 ℃; Inert atmosphere;

3-(benzyloxy)propyl trifluoromethanesulfonate; In tetrahydrofuran; toluene; at -78 ℃; for 1h; Inert atmosphere;
DOI:10.1021/ol202629d