1-<<(4-methylphenyl)sulfonyl>oxy>-4-nitro-5,8-bis(phenylmethoxy)-9,10-anthracenedione

Base Information

Chemical Name:1-<<(4-methylphenyl)sulfonyl>oxy>-4-nitro-5,8-bis(phenylmethoxy)-9,10-anthracenedione
CAS No.:154160-39-1
Molecular Formula:C₃₅H₂₅NO₉S
Molecular Weight:635.651
Hs Code.:

Synonyms:1-<<(4-methylphenyl)sulfonyl>oxy>-4-nitro-5,8-bis(phenylmethoxy)-9,10-anthracenedione

Suppliers and Price of 1-<<(4-methylphenyl)sulfonyl>oxy>-4-nitro-5,8-bis(phenylmethoxy)-9,10-anthracenedione

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 1-<<(4-methylphenyl)sulfonyl>oxy>-4-nitro-5,8-bis(phenylmethoxy)-9,10-anthracenedione

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 1-<<(4-methylphenyl)sulfonyl>oxy>-4-nitro-5,8-bis(phenylmethoxy)-9,10-anthracenedione

There total 2 articles about 1-<<(4-methylphenyl)sulfonyl>oxy>-4-nitro-5,8-bis(phenylmethoxy)-9,10-anthracenedione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 98-59-9
p-toluenesulfonyl chloride

: 154160-38-0
1-hydroxy-4-nitro-5,8-bis(phenylmethoxy)-9,10-anthracenedione

: 154160-39-1
1-<<(4-methylphenyl)sulfonyl>oxy>-4-nitro-5,8-bis(phenylmethoxy)-9,10-anthracenedione

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In acetonitrile; at 5 ℃; for 18h;
DOI:10.1002/jhet.5570300236

Reference yield:

: 91440-79-8
1,4-di(benzyloxy)-5,8-dichloro-9,10-dihydro-9,10-anthracenedione

: 154160-39-1
1-<<(4-methylphenyl)sulfonyl>oxy>-4-nitro-5,8-bis(phenylmethoxy)-9,10-anthracenedione

Guidance literature:: Multi-step reaction with 2 steps

1: 65 percent / NaNO₂, KF / N,N-dimethyl-acetamide / 5 h / 155 °C

2: 81 percent / N,N-diisopropylethylamine / acetonitrile / 18 h / 5 °C

With potassium fluoride; N-ethyl-N,N-diisopropylamine; sodium nitrite; In N,N-dimethyl acetamide; acetonitrile;
DOI:10.1002/jhet.5570300236