5-O-benzyl-3-O-[tert-butyl(diphenyl)silyl]-2,4-dideoxy-4-methyl-D-erythro-pentose

Base Information

Chemical Name:5-O-benzyl-3-O-[tert-butyl(diphenyl)silyl]-2,4-dideoxy-4-methyl-D-erythro-pentose
CAS No.:1092368-84-7
Molecular Formula:C₂₉H₃₆O₃Si
Molecular Weight:460.689
Hs Code.:

Synonyms:5-O-benzyl-3-O-[tert-butyl(diphenyl)silyl]-2,4-dideoxy-4-methyl-D-erythro-pentose

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 5-O-benzyl-3-O-[tert-butyl(diphenyl)silyl]-2,4-dideoxy-4-methyl-D-erythro-pentose

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Technology Process of 5-O-benzyl-3-O-[tert-butyl(diphenyl)silyl]-2,4-dideoxy-4-methyl-D-erythro-pentose

There total 1 articles about 5-O-benzyl-3-O-[tert-butyl(diphenyl)silyl]-2,4-dideoxy-4-methyl-D-erythro-pentose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.6%

: 1092368-83-6
{[(2R,3S)-1-(benzyloxy)-2-methylhex-5-en-3-yl]oxy}(tert-butyl)diphenylsilane

: 1092368-84-7
5-O-benzyl-3-O-[tert-butyl(diphenyl)silyl]-2,4-dideoxy-4-methyl-D-erythro-pentose

Guidance literature:: With 2,6-dimethylpyridine; sodium periodate; osmium(VIII) oxide; In 1,4-dioxane; water; tert-butyl alcohol; at 25 ℃; for 5h; Inert atmosphere;
DOI:10.1055/s-0029-1216903

Reference yield: 93.0%

: 1092368-84-7
5-O-benzyl-3-O-[tert-butyl(diphenyl)silyl]-2,4-dideoxy-4-methyl-D-erythro-pentose

: 101711-78-8,131685-53-5
(3R)-3-propionyl-4-benzyloxazolidin-2-one

: 1092368-85-8
(4R)-4-benzyl-3-[(2R,3S,5S,6R)-7-(benzyloxy)-5-{[tert-butyl(diphenyl)silyl]oxy}-3-hydroxy-2,6-dimethylheptanoyl]-1,3-oxazolidin-2-one

Guidance literature:: (3R)-3-propionyl-4-benzyloxazolidin-2-one; With titanium tetrachloride; (-)-sparteine; In dichloromethane; at 0 ℃; for 0.416667h; Inert atmosphere;

5-O-benzyl-3-O-[tert-butyl(diphenyl)silyl]-2,4-dideoxy-4-methyl-D-erythro-pentose; In dichloromethane; at 0 ℃; for 1h;
DOI:10.1055/s-0029-1216903