1,4,5,6,7,7-Hexachlorobicyclo[2.2.1]hept-5-ene-2,3-dicarboxylic acid diethyl ester

Base Information

• Chemical Name: 1,4,5,6,7,7-Hexachlorobicyclo[2.2.1]hept-5-ene-2,3-dicarboxylic acid diethyl ester
• CAS No.: 1911-42-8
• Molecular Formula: C13H12Cl6O4
• Molecular Weight: 444.95
• Mol file: 1911-42-8.mol

Synonyms:1,4,5,6,7,7-Hexachloro-5-norbornene-2,3-dicarboxylic acid diethyl ester;Chlorendic acid,diethyl ester;1,4,5,6,7,7-Hexachloro-5-norbornene-2,3-dicarboxylic acid diethyl;5-Norbornene-2,3-dicarboxylic acid,1,4,5,6,7,7-hexachloro-,diethyl ester;

Chemical Property of 1,4,5,6,7,7-Hexachlorobicyclo[2.2.1]hept-5-ene-2,3-dicarboxylic acid diethyl ester

Chemical Property:

• Vapor Pressure: 2.19E-08mmHg at 25°C
• Boiling Point: 452.7°Cat760mmHg
• Flash Point: 163.4°C
• PSA: 52.60000
• Density: 1.61g/cm³
• LogP: 4.19050

Purity/Quality:

98%,99%, ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 1,4,5,6,7,7-Hexachlorobicyclo[2.2.1]hept-5-ene-2,3-dicarboxylic acid diethyl ester

There total 4 articles about 1,4,5,6,7,7-Hexachlorobicyclo[2.2.1]hept-5-ene-2,3-dicarboxylic acid diethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

Diethyl maleate (141-05-9) + hexachlorocyclopentadiene (77-47-4) → 1.4.5.6.7.7-hexachloro-norbornene-(5)-dicarboxylic acid-(2endo.3endo)-diethyl ester (1911-42-8)

Guidance literature:

at 100 ℃;

DOI:10.1021/ja01193a015

Reference yield:

1,2,3,4,7,7-hexachlorobicyclo[2.2.1]hept-2-ene-endo-cis-5,6-dicarboxylic acid (21678-54-6,316187-04-9,7374-78-9) → 1.4.5.6.7.7-hexachloro-norbornene-(5)-dicarboxylic acid-(2endo.3endo)-diethyl ester (1911-42-8)

Guidance literature:

Reference yield:

→ 1,4,5,6,7,7-Hexachlor-bicyclo<2.2.1>hepten-(5)-dicarbonsaeure-(2,3)-diaethylester (1911-42-8)

Guidance literature:

Anhydrid von 1,4,5,6,7,7-Hexachlor-bicyclo<2.2.1>hepten-(5)-dicarbonsaeure-(2,3), H2SO4, A.;

upstream raw materials:

1,2,3,4,7,7-hexachlorobicyclo[2.2.1]hept-2-ene-endo-cis-5,6-dicarboxylic acid

Diethyl maleate

hexachlorocyclopentadiene