D-3-O-[S-(+)-O-Acetylmandelyl]-6-deoxy-1,4,5-tri-O-p-methoxybenzyl-myo-inositol

Base Information

Chemical Name:D-3-O-[S-(+)-O-Acetylmandelyl]-6-deoxy-1,4,5-tri-O-p-methoxybenzyl-myo-inositol
CAS No.:328379-85-7
Molecular Formula:C₄₀H₄₄O₁₁
Molecular Weight:700.783
Hs Code.:

Synonyms:D-3-O-[S-(+)-O-Acetylmandelyl]-6-deoxy-1,4,5-tri-O-p-methoxybenzyl-myo-inositol

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Chemical Property of D-3-O-[S-(+)-O-Acetylmandelyl]-6-deoxy-1,4,5-tri-O-p-methoxybenzyl-myo-inositol

Chemical Property:

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Technology Process of D-3-O-[S-(+)-O-Acetylmandelyl]-6-deoxy-1,4,5-tri-O-p-methoxybenzyl-myo-inositol

There total 3 articles about D-3-O-[S-(+)-O-Acetylmandelyl]-6-deoxy-1,4,5-tri-O-p-methoxybenzyl-myo-inositol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 40.0%

: 7322-88-5
(S)-acetylmandelic acid

: DL-6-Deoxy-1,4,5-tri-O-p-methoxybenzyl-myo-inositol

: 328379-86-8
L-3-O-[S-(+)-O-Acetylmandelyl]-6-deoxy-1,4,5-tri-O-p-methoxybenzyl-myo-inositol

: 328379-85-7
D-3-O-[S-(+)-O-Acetylmandelyl]-6-deoxy-1,4,5-tri-O-p-methoxybenzyl-myo-inositol

Guidance literature:: With dmap; dicyclohexyl-carbodiimide; In dichloromethane; at -20 ℃;
DOI:10.1002/1521-3765(20010105)7:1<80::AID-CHEM80>3.0.CO;2-B

Reference yield:

: DL-6-Deoxy-2,3-O-isopropylidene-1,4,5-tri-O-p-methoxybenzyl-myo-inositol

: 328379-85-7
D-3-O-[S-(+)-O-Acetylmandelyl]-6-deoxy-1,4,5-tri-O-p-methoxybenzyl-myo-inositol

Guidance literature:: Multi-step reaction with 2 steps

1: 77 percent / aq. AcOH / 0.5 h / 50 °C

2: 38 percent / DMAP; DCC / CH₂Cl₂ / -20 °C

With dmap; acetic acid; dicyclohexyl-carbodiimide; In dichloromethane;
DOI:10.1002/1521-3765(20010105)7:1<80::AID-CHEM80>3.0.CO;2-B

Reference yield:

: Dithiocarbonic acid S-methyl ester O-[(3aS,4S,5R,6S,7S,7aS)-5,6,7-tris-(4-methoxy-benzyloxy)-2,2-dimethyl-hexahydro-benzo[1,3]dioxol-4-yl] ester

: 328379-85-7
D-3-O-[S-(+)-O-Acetylmandelyl]-6-deoxy-1,4,5-tri-O-p-methoxybenzyl-myo-inositol

Guidance literature:: Multi-step reaction with 3 steps

1: 4.03 g / Bu₃SnH; AIBN / toluene / 1 h / Heating

2: 77 percent / aq. AcOH / 0.5 h / 50 °C

3: 38 percent / DMAP; DCC / CH₂Cl₂ / -20 °C

With dmap; 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride; acetic acid; dicyclohexyl-carbodiimide; In dichloromethane; toluene; 1: Barton-McCombie reaction;
DOI:10.1002/1521-3765(20010105)7:1<80::AID-CHEM80>3.0.CO;2-B