ethyl 2-[(diphenylacetyl)amino]-4,5,6,7-tetrahydro-1-benzothiophene-3-carboxylate

Base Information

• Chemical Name: ethyl 2-[(diphenylacetyl)amino]-4,5,6,7-tetrahydro-1-benzothiophene-3-carboxylate
• CAS No.: 79750-91-7
• Molecular Formula: C₂₅H₂₅NO₃S
• Molecular Weight: 419.544
• Mol file: 79750-91-7.mol

Synonyms:2-Diphenylacetylamino-4,5,6,7-tetrahydrobenzothiophen-3-carbonsaeure-ethylester

Chemical Property of ethyl 2-[(diphenylacetyl)amino]-4,5,6,7-tetrahydro-1-benzothiophene-3-carboxylate

Chemical Property:

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Technology Process of ethyl 2-[(diphenylacetyl)amino]-4,5,6,7-tetrahydro-1-benzothiophene-3-carboxylate

There total 1 articles about ethyl 2-[(diphenylacetyl)amino]-4,5,6,7-tetrahydro-1-benzothiophene-3-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

diphenylacetic acid chloride (1871-76-7) + ethyl 2-amino-4,5,6,7-tetrahydrobenzo[b]thiophene-3-carboxylate (4506-71-2) → 2-Diphenylacetylamino-4,5,6,7-tetrahydrobenzothiophen-3-carbonsaeure-ethylester (79750-91-7)

Guidance literature:

With triethylamine; In benzene; for 1h; Heating;

Reference yield: 95.0%

2-Diphenylacetylamino-4,5,6,7-tetrahydrobenzothiophen-3-carbonsaeure-ethylester (79750-91-7) → 2-Diphenylmethyl-5,6,7,8-tetrahydro-4H-<1>benzothieno<2,3-d><1,3>oxazin-4-on (79750-95-1)

Guidance literature:

With hexachloroethane; triethylamine; triphenylphosphine; In dichloromethane; for 2h; Heating;

upstream raw materials:

diphenylacetic acid chloride

ethyl 2-amino-4,5,6,7-tetrahydrobenzo[b]thiophene-3-carboxylate

Downstream raw materials:

2-Diphenylmethyl-5,6,7,8-tetrahydro-4H-<1>benzothieno<2,3-d><1,3>oxazin-4-on

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