tert-butyl tert-butyloxycarbonyl-L-phenylalanyl-L-4-aminophenylalaninate

Base Information

Chemical Name:tert-butyl tert-butyloxycarbonyl-L-phenylalanyl-L-4-aminophenylalaninate
CAS No.:320782-46-5
Molecular Formula:C₂₇H₃₇N₃O₅
Molecular Weight:483.608
Hs Code.:

Synonyms:tert-butyl tert-butyloxycarbonyl-L-phenylalanyl-L-4-aminophenylalaninate

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Chemical Property of tert-butyl tert-butyloxycarbonyl-L-phenylalanyl-L-4-aminophenylalaninate

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Technology Process of tert-butyl tert-butyloxycarbonyl-L-phenylalanyl-L-4-aminophenylalaninate

There total 3 articles about tert-butyl tert-butyloxycarbonyl-L-phenylalanyl-L-4-aminophenylalaninate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: tert-butyl tert-butyloxycarbonyl-L-phenylalanyl-L-4-nitrophenylalaninate

: 320782-46-5
tert-butyl tert-butyloxycarbonyl-L-phenylalanyl-L-4-aminophenylalaninate

Guidance literature:: With ammonium formate; 10percent Pd/C; In methanol; water; for 0.5h;
DOI:10.1021/jm000345s

Reference yield:

: 13734-34-4
N-tert-butoxycarbonyl-L-phenylalanine

: 320782-46-5
tert-butyl tert-butyloxycarbonyl-L-phenylalanyl-L-4-aminophenylalaninate

Guidance literature:: Multi-step reaction with 2 steps

1: 73 percent / N-methylmorpholine / dimethylformamide / -15 - 20 °C

2: 97 percent / HCOONH₄ / 10percent Pd/C / methanol; H₂O / 0.5 h

With 4-methyl-morpholine; ammonium formate; 10percent Pd/C; In methanol; water; N,N-dimethyl-formamide;
DOI:10.1021/jm000345s

Reference yield:

: 116366-32-6
L-4-nitrophenylalanine tert-butyl ester

: 320782-46-5
tert-butyl tert-butyloxycarbonyl-L-phenylalanyl-L-4-aminophenylalaninate

Guidance literature:: Multi-step reaction with 2 steps

1: 73 percent / N-methylmorpholine / dimethylformamide / -15 - 20 °C

2: 97 percent / HCOONH₄ / 10percent Pd/C / methanol; H₂O / 0.5 h

With 4-methyl-morpholine; ammonium formate; 10percent Pd/C; In methanol; water; N,N-dimethyl-formamide;
DOI:10.1021/jm000345s