1-benzyl-3-<2-(1,3-dithiolanyl)>-9-methoxy-1H-benzindole

Base Information

Chemical Name:1-benzyl-3-<2-(1,3-dithiolanyl)>-9-methoxy-1H-benzindole
CAS No.:151646-91-2
Molecular Formula:C₂₃H₂₁NOS₂
Molecular Weight:391.558
Hs Code.:

1-benzyl-3-<2-(1,3-dithiolanyl)>-9-methoxy-1H-benz<f>indole

Synonyms:1-benzyl-3-<2-(1,3-dithiolanyl)>-9-methoxy-1H-benzindole

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-benzyl-3-<2-(1,3-dithiolanyl)>-9-methoxy-1H-benzindole

Chemical Property:

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Technology Process of 1-benzyl-3-<2-(1,3-dithiolanyl)>-9-methoxy-1H-benzindole

There total 4 articles about 1-benzyl-3-<2-(1,3-dithiolanyl)>-9-methoxy-1H-benzindole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 540-63-6
ethane-1,2-dithiol

: 151646-90-1
1-benzyl-3-formyl-9-methoxy-1H-benzindole

: 151646-91-2
1-benzyl-3-<2-(1,3-dithiolanyl)>-9-methoxy-1H-benzindole

Guidance literature:: With boron trifluoride diethyl etherate; In acetic acid; for 0.75h; Ambient temperature;
DOI:10.1002/jhet.5570300137

Reference yield:

: 121045-66-7
ethyl 1-benzyl-9-methoxy-1H-benzindole-2-carboxylate

: 151646-91-2
1-benzyl-3-<2-(1,3-dithiolanyl)>-9-methoxy-1H-benzindole

Guidance literature:: Multi-step reaction with 4 steps

1: KOH / ethanol / 0.5 h / Heating

2: copper chromite / quinoline / 0.25 h / 200 °C

3: 69 percent / phosphoryl chloride / 0.5 h / 0 °C

4: 100 percent / boron trifluoride-etherate / acetic acid / 0.75 h / Ambient temperature

With potassium hydroxide; copper chromite; boron trifluoride diethyl etherate; trichlorophosphate; In quinoline; ethanol; acetic acid;
DOI:10.1002/jhet.5570300137

Reference yield:

: 151646-89-8
1-benzyl-9-methoxy-1H-benzindole

: 151646-91-2
1-benzyl-3-<2-(1,3-dithiolanyl)>-9-methoxy-1H-benzindole

Guidance literature:: Multi-step reaction with 2 steps

1: 69 percent / phosphoryl chloride / 0.5 h / 0 °C

2: 100 percent / boron trifluoride-etherate / acetic acid / 0.75 h / Ambient temperature

With boron trifluoride diethyl etherate; trichlorophosphate; In acetic acid;
DOI:10.1002/jhet.5570300137