1,4,7,10,14-pentatosyl-1,4,7,10,14-pentaazacycloheptadecane

Base Information

• Chemical Name: 1,4,7,10,14-pentatosyl-1,4,7,10,14-pentaazacycloheptadecane
• CAS No.: 108603-01-6
• Molecular Formula: C₄₇H₅₉N₅O₁₀S₅
• Molecular Weight: 1014.34
• Mol file: 108603-01-6.mol

Synonyms:1,4,7,10,14-pentatosyl-1,4,7,10,14-pentaazacycloheptadecane

Chemical Property of 1,4,7,10,14-pentatosyl-1,4,7,10,14-pentaazacycloheptadecane

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 1,4,7,10,14-pentatosyl-1,4,7,10,14-pentaazacycloheptadecane

There total 3 articles about 1,4,7,10,14-pentatosyl-1,4,7,10,14-pentaazacycloheptadecane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

1,8-bis(p-toluenesulfonyloxy)-3,6-bis(p-toluenesulfonyl)-3,6-diazaoctane (56234-52-7) + 1,5,9-Tritosyl-1,5,9-triazanonane (35980-64-4) → 1,4,7,10,14-pentatosyl-1,4,7,10,14-pentaazacycloheptadecane (108603-01-6)

Guidance literature:

With sodium hydroxide; tetra-(n-butyl)ammonium iodide; In water; toluene; Heating; 8-10 h;

DOI:10.1007/BF00472559

Reference yield: 82.0%

disodium 1,4,7,10-tetrakis(p-tolylsulfonyl)-1,4,7,10-tetraazadecane-N,N'''-diide (56187-06-5,99892-33-8) + 3,3'-(tosylimino)bispropyl ditosylate → 1,4,7,10,14-pentatosyl-1,4,7,10,14-pentaazacycloheptadecane (108603-01-6)

Guidance literature:

at 100 ℃;

Reference yield: 56.0%

→ 1,4,7,10,14-pentatosyl-1,4,7,10,14-pentaazacycloheptadecane (108603-01-6)

Guidance literature:

upstream raw materials:

1,8-bis(p-toluenesulfonyloxy)-3,6-bis(p-toluenesulfonyl)-3,6-diazaoctane

1,5,9-Tritosyl-1,5,9-triazanonane

disodium 1,4,7,10-tetrakis(p-tolylsulfonyl)-1,4,7,10-tetraazadecane-N,N'''-diide