Technology Process of C31H30N2O2S
There total 4 articles about C31H30N2O2S which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
indium(III) chloride;
In
acetonitrile;
at 20 ℃;
for 0.166667h;
diastereoselective reaction;
DOI:10.1080/00397911.2011.572218
- Guidance literature:
-
Multi-step reaction with 3 steps
1: potassium carbonate / acetone / Inert atmosphere
2: 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione / dimethyl sulfoxide / 2 h
3: indium(III) chloride / acetonitrile / 0.17 h / 20 °C
With
indium(III) chloride; potassium carbonate; 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione;
In
dimethyl sulfoxide; acetone; acetonitrile;
3: Imino Diels-Alder reaction;
DOI:10.1080/00397911.2011.572218
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: sodium tetrahydroborate / ethanol; water / 4.5 h / Reflux
2.1: benzene / 0.17 h / 0 °C
2.2: 20 °C
3.1: potassium carbonate / acetone / Inert atmosphere
4.1: 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione / dimethyl sulfoxide / 2 h
5.1: indium(III) chloride / acetonitrile / 0.17 h / 20 °C
With
indium(III) chloride; sodium tetrahydroborate; potassium carbonate; 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione;
In
ethanol; water; dimethyl sulfoxide; acetone; acetonitrile; benzene;
5.1: Imino Diels-Alder reaction;
DOI:10.1080/00397911.2011.572218
