C₁₇H₂₄O₆

Base Information

Chemical Name:C₁₇H₂₄O₆
CAS No.:1301166-63-1
Molecular Formula:C₁₇H₂₄O₆
Molecular Weight:324.374
Hs Code.:

C<sub>17</sub>H<sub>24</sub>O<sub>6</sub>

Synonyms:C₁₇H₂₄O₆

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Chemical Property of C₁₇H₂₄O₆

Chemical Property:

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Technology Process of C₁₇H₂₄O₆

There total 9 articles about C₁₇H₂₄O₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 1301166-55-1
C₁₇H₂₆O₆

: 1301166-63-1
C₁₇H₂₄O₆

Guidance literature:: With 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione; In dichloromethane; dimethyl sulfoxide; at 20 ℃; for 3h;
DOI:10.1016/j.tetlet.2011.02.025

Reference yield:

: 1301166-51-7
C₁₀H₁₈O₅

: 1301166-63-1
C₁₇H₂₄O₆

Guidance literature:: Multi-step reaction with 5 steps

1.1: Nitrosobenzene; D-Prolin / dimethyl sulfoxide

1.2: 0.5 h

2.1: 1H-imidazole / dichloromethane / 1 h

3.1: tetra-(n-butyl)ammonium iodide; sodium hydride / tetrahydrofuran / 2 h / 0 - 20 °C

4.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 0 - 20 °C

5.1: 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione / dichloromethane; dimethyl sulfoxide / 3 h / 20 °C

With 1H-imidazole; tetrabutyl ammonium fluoride; tetra-(n-butyl)ammonium iodide; sodium hydride; Nitrosobenzene; D-Prolin; 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione; In tetrahydrofuran; dichloromethane; dimethyl sulfoxide; 1.1: MacMillan α-hydroxylation / 1.2: MacMillan α-hydroxylation / 1.3: MacMillan α-hydroxylation;
DOI:10.1016/j.tetlet.2011.02.025

Reference yield:

: C₁₁H₂₂O₆

: 1301166-63-1
C₁₇H₂₄O₆

Guidance literature:: Multi-step reaction with 6 steps

1.1: sodium periodate / 2 h / 20 °C

2.1: Nitrosobenzene; D-Prolin / dimethyl sulfoxide

2.2: 0.5 h

3.1: 1H-imidazole / dichloromethane / 1 h

4.1: tetra-(n-butyl)ammonium iodide; sodium hydride / tetrahydrofuran / 2 h / 0 - 20 °C

5.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 0 - 20 °C

6.1: 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione / dichloromethane; dimethyl sulfoxide / 3 h / 20 °C

With 1H-imidazole; sodium periodate; tetrabutyl ammonium fluoride; tetra-(n-butyl)ammonium iodide; sodium hydride; Nitrosobenzene; D-Prolin; 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione; In tetrahydrofuran; dichloromethane; dimethyl sulfoxide; 2.1: MacMillan α-hydroxylation / 2.2: MacMillan α-hydroxylation / 2.3: MacMillan α-hydroxylation;
DOI:10.1016/j.tetlet.2011.02.025