C₃₀H₄₈N₂O₆Si

Base Information

Chemical Name:C₃₀H₄₈N₂O₆Si
CAS No.:1395688-64-8
Molecular Formula:C₃₀H₄₈N₂O₆Si
Molecular Weight:560.806
Hs Code.:

C<sub>30</sub>H<sub>48</sub>N<sub>2</sub>O<sub>6</sub>Si

Synonyms:C₃₀H₄₈N₂O₆Si

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Chemical Property of C₃₀H₄₈N₂O₆Si

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Technology Process of C₃₀H₄₈N₂O₆Si

There total 17 articles about C₃₀H₄₈N₂O₆Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 24424-99-5
di-tert-butyl dicarbonate

: 1395688-56-8
C₃₂H₄₄N₄O₄Si

: 1395688-64-8
C₃₀H₄₈N₂O₆Si

Guidance literature:: C₃₂H₄₄N₄O₄Si; With palladium 10% on activated carbon; hydrogen; under 760.051 Torr;

di-tert-butyl dicarbonate; In methanol;
DOI:10.1021/jo302362b

Reference yield:

: 1395687-54-3
(R)-1-allyl-5-(benzyloxy)piperidin-2-one

: 1395688-64-8
C₃₀H₄₈N₂O₆Si

Guidance literature:: Multi-step reaction with 15 steps

1.1: trifluoromethylsulfonic anhydride; 2,6-di-tert-butyl-4-methylpyridine / dichloromethane

2.1: lithium naphthalenide / tetrahydrofuran / 1 h / -40 °C

3.1: oxalyl dichloride; dimethyl sulfoxide / dichloromethane / 1 h / -78 °C

4.1: hydrogenchloride / tetrahydrofuran; water / 1.5 h / 20 - 50 °C

4.3: CSA / 0.17 h / 90 °C

5.1: sodium hydride; tetra-(n-butyl)ammonium iodide / N,N-dimethyl-formamide / 18 h / 20 °C

6.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾ / dichloromethane / 1 h / 20 °C

7.1: triethylamine / dichloromethane / 0.5 h / 0 °C

8.1: titanium(IV) isopropylate; tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride / toluene / 12 h / 85 °C

9.1: hydrogenchloride / acetone / 3 h / Reflux

10.1: potassium hexamethylsilazane / tetrahydrofuran / -50 °C

10.2: 0 °C

11.1: palladium 10% on activated carbon; hydrogen / ethyl acetate / 3 h / 20 °C / 760.05 Torr

12.1: samarium diiodide; N,N,N,N,N,N-hexamethylphosphoric triamide / methanol / 12 h / -78 °C

13.1: triethylamine / dichloromethane / 3 h / 20 °C

14.1: lithium diisopropyl amide / tetrahydrofuran / 0.08 h / -78 °C

15.1: palladium 10% on activated carbon; hydrogen / 760.05 Torr

With tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; titanium(IV) isopropylate; hydrogenchloride; N,N,N,N,N,N-hexamethylphosphoric triamide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; 2,6-di-tert-butyl-4-methylpyridine; samarium diiodide; oxalyl dichloride; trifluoromethylsulfonic anhydride; palladium 10% on activated carbon; hydrogen; tetra-(n-butyl)ammonium iodide; potassium hexamethylsilazane; sodium hydride; dimethyl sulfoxide; triethylamine; lithium diisopropyl amide; In tetrahydrofuran; methanol; dichloromethane; water; ethyl acetate; N,N-dimethyl-formamide; acetone; toluene; 3.1: |Swern Oxidation / 3.2: |Swern Oxidation;
DOI:10.1021/jo302362b

Reference yield:

: 1395687-70-3
(3R,6R)-6-[2-(1,3-dioxolan-2-yl)ethyl]-1-allyl-6-vinylpiperidin-3-ol

: 1395688-64-8
C₃₀H₄₈N₂O₆Si

Guidance literature:: Multi-step reaction with 13 steps

1.1: oxalyl dichloride; dimethyl sulfoxide / dichloromethane / 1 h / -78 °C

2.1: hydrogenchloride / tetrahydrofuran; water / 1.5 h / 20 - 50 °C

2.3: CSA / 0.17 h / 90 °C

3.1: sodium hydride; tetra-(n-butyl)ammonium iodide / N,N-dimethyl-formamide / 18 h / 20 °C

4.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾ / dichloromethane / 1 h / 20 °C

5.1: triethylamine / dichloromethane / 0.5 h / 0 °C

6.1: titanium(IV) isopropylate; tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride / toluene / 12 h / 85 °C

7.1: hydrogenchloride / acetone / 3 h / Reflux

8.1: potassium hexamethylsilazane / tetrahydrofuran / -50 °C

8.2: 0 °C

9.1: palladium 10% on activated carbon; hydrogen / ethyl acetate / 3 h / 20 °C / 760.05 Torr

10.1: samarium diiodide; N,N,N,N,N,N-hexamethylphosphoric triamide / methanol / 12 h / -78 °C

11.1: triethylamine / dichloromethane / 3 h / 20 °C

12.1: lithium diisopropyl amide / tetrahydrofuran / 0.08 h / -78 °C

13.1: palladium 10% on activated carbon; hydrogen / 760.05 Torr

With tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; titanium(IV) isopropylate; hydrogenchloride; N,N,N,N,N,N-hexamethylphosphoric triamide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; samarium diiodide; oxalyl dichloride; palladium 10% on activated carbon; hydrogen; tetra-(n-butyl)ammonium iodide; potassium hexamethylsilazane; sodium hydride; dimethyl sulfoxide; triethylamine; lithium diisopropyl amide; In tetrahydrofuran; methanol; dichloromethane; water; ethyl acetate; N,N-dimethyl-formamide; acetone; toluene; 1.1: |Swern Oxidation / 1.2: |Swern Oxidation;
DOI:10.1021/jo302362b