(2S,3S)-4-methoxybenzyl 2-(((4-methoxyphenyl)thio)carbonyl)-2-methyl-4-nitro-3-phenylbutanoate

Base Information

• Chemical Name: (2S,3S)-4-methoxybenzyl 2-(((4-methoxyphenyl)thio)carbonyl)-2-methyl-4-nitro-3-phenylbutanoate
• CAS No.: 1603832-45-6
• Molecular Formula: C₂₇H₂₇NO₇S
• Molecular Weight: 509.58

Synonyms:(2S,3S)-4-methoxybenzyl 2-(((4-methoxyphenyl)thio)carbonyl)-2-methyl-4-nitro-3-phenylbutanoate

Chemical Property of (2S,3S)-4-methoxybenzyl 2-(((4-methoxyphenyl)thio)carbonyl)-2-methyl-4-nitro-3-phenylbutanoate

Chemical Property:

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Technology Process of (2S,3S)-4-methoxybenzyl 2-(((4-methoxyphenyl)thio)carbonyl)-2-methyl-4-nitro-3-phenylbutanoate

There total 2 articles about (2S,3S)-4-methoxybenzyl 2-(((4-methoxyphenyl)thio)carbonyl)-2-methyl-4-nitro-3-phenylbutanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

nitrostyrene (5153-67-3) + 4-methoxybenzyl 3-[(4-methoxyphenyl)sulfanyl]-2-methyl-3-oxopropanoate (1603833-09-5) → (2S,3S)-4-methoxybenzyl 2-(((4-methoxyphenyl)thio)carbonyl)-2-methyl-4-nitro-3-phenylbutanoate (1603832-45-6) + 4-methoxybenzyl 2-(((4-methoxyphenyl)thio)carbonyl)-2-methyl-4-nitro-3-phenylbutanoate + 4-methoxybenzyl 2-(((4-methoxyphenyl)thio)carbonyl)-2-methyl-4-nitro-3-phenylbutanoate

Guidance literature:

With quinine; In toluene; at 20 ℃; enantioselective reaction;

DOI:10.1021/jo500403q

Reference yield:

nitrostyrene (5153-67-3) + 4-methoxybenzyl 3-[(4-methoxyphenyl)sulfanyl]-2-methyl-3-oxopropanoate (1603833-09-5) → (2S,3S)-4-methoxybenzyl 2-(((4-methoxyphenyl)thio)carbonyl)-2-methyl-4-nitro-3-phenylbutanoate (1603832-45-6) + 4-methoxybenzyl 2-(((4-methoxyphenyl)thio)carbonyl)-2-methyl-4-nitro-3-phenylbutanoate

Guidance literature:

With 1-(3,5-bis(trifluoromethyl)phenyl)-3-[(R)-(quinolin-4-yl)((2R,4S,5R)-5-vinylquinuclidin-2-yl)methyl]urea; In toluene; at -15 ℃; for 24h; Reagent/catalyst; Temperature; Solvent; Time; Overall yield = 87 %; Overall yield = 89 mg; enantioselective reaction; Catalytic behavior;

DOI:10.1021/jo500403q

Reference yield: 67.0%

(2S,3S)-4-methoxybenzyl 2-(((4-methoxyphenyl)thio)carbonyl)-2-methyl-4-nitro-3-phenylbutanoate (1603832-45-6) → 4-methoxybenzyl (2R,3S)-2-formyl-2-methyl-4-nitro-3-phenylbutanoate (1603832-82-1)

Guidance literature:

With triethylsilane; palladium 10% on activated carbon; In acetone; at 20 ℃; for 4h;

DOI:10.1021/jo500403q

upstream raw materials:

nitrostyrene

4-methoxybenzyl 3-[(4-methoxyphenyl)sulfanyl]-2-methyl-3-oxopropanoate

Downstream raw materials:

4-methoxybenzyl (2R,3S)-2-formyl-2-methyl-4-nitro-3-phenylbutanoate

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