4-{[4-({4-[(trimethylsilyl)ethynyl]phenyl}ethynyl)phenyl]ethynyl}benzenaminium chloride

Base Information

Chemical Name:4-{[4-({4-[(trimethylsilyl)ethynyl]phenyl}ethynyl)phenyl]ethynyl}benzenaminium chloride
CAS No.:1589009-86-8
Molecular Formula:C₂₇H₂₃NSi*ClH
Molecular Weight:426.033
Hs Code.:

Synonyms:4-{[4-({4-[(trimethylsilyl)ethynyl]phenyl}ethynyl)phenyl]ethynyl}benzenaminium chloride

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Chemical Property of 4-{[4-({4-[(trimethylsilyl)ethynyl]phenyl}ethynyl)phenyl]ethynyl}benzenaminium chloride

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Technology Process of 4-{[4-({4-[(trimethylsilyl)ethynyl]phenyl}ethynyl)phenyl]ethynyl}benzenaminium chloride

There total 3 articles about 4-{[4-({4-[(trimethylsilyl)ethynyl]phenyl}ethynyl)phenyl]ethynyl}benzenaminium chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 910467-54-8
4-((4-((4-((trimethylsilyl)ethynyl)phenyl)ethynyl)phenyl)ethynyl)aniline

: 1589009-86-8
4-{[4-({4-[(trimethylsilyl)ethynyl]phenyl}ethynyl)phenyl]ethynyl}benzenaminium chloride

Guidance literature:: With hydrogenchloride; In dichloromethane; at 20 ℃; for 3h; Inert atmosphere; Schlenk technique;
DOI:10.1002/chem.201303967

Reference yield:

: 66228-76-0
4-(trimethylsilylethynyl)phenylacetylene

: 1589009-86-8
4-{[4-({4-[(trimethylsilyl)ethynyl]phenyl}ethynyl)phenyl]ethynyl}benzenaminium chloride

Guidance literature:: Multi-step reaction with 3 steps

1: copper(l) iodide; triethylamine; tetrakis(triphenylphosphine) palladium⁽⁰⁾ / 5 h / 0 °C / Inert atmosphere; Schlenk technique

2: Inert atmosphere; Schlenk technique; Reflux

3: hydrogenchloride / dichloromethane / 3 h / 20 °C / Inert atmosphere; Schlenk technique

With hydrogenchloride; copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; triethylamine; In dichloromethane;
DOI:10.1002/chem.201303967

Reference yield:

: 589-87-7
1,4-bromoiodobenzene

: 1589009-86-8
4-{[4-({4-[(trimethylsilyl)ethynyl]phenyl}ethynyl)phenyl]ethynyl}benzenaminium chloride

Guidance literature:: Multi-step reaction with 3 steps

1: copper(l) iodide; triethylamine; tetrakis(triphenylphosphine) palladium⁽⁰⁾ / 5 h / 0 °C / Inert atmosphere; Schlenk technique

2: Inert atmosphere; Schlenk technique; Reflux

3: hydrogenchloride / dichloromethane / 3 h / 20 °C / Inert atmosphere; Schlenk technique

With hydrogenchloride; copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; triethylamine; In dichloromethane;
DOI:10.1002/chem.201303967