(N,N'-bis-2,6-diisopropylphenyl-2,4-dimethyl-1,5-diketamide)Cu(acetonitrile)

Base Information

• Chemical Name: (N,N'-bis-2,6-diisopropylphenyl-2,4-dimethyl-1,5-diketamide)Cu(acetonitrile)
• CAS No.: 410527-15-0
• Molecular Formula: C₃₁H₄₄CuN₃
• Molecular Weight: 522.256

Synonyms:(N,N'-bis-2,6-diisopropylphenyl-2,4-dimethyl-1,5-diketamide)Cu(acetonitrile)

Chemical Property of (N,N'-bis-2,6-diisopropylphenyl-2,4-dimethyl-1,5-diketamide)Cu(acetonitrile)

Chemical Property:

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Technology Process of (N,N'-bis-2,6-diisopropylphenyl-2,4-dimethyl-1,5-diketamide)Cu(acetonitrile)

There total 5 articles about (N,N'-bis-2,6-diisopropylphenyl-2,4-dimethyl-1,5-diketamide)Cu(acetonitrile) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

N,N′-bis(2,6-diisopropylphenyl)pentane-2,4-diimine (210832-39-6) + tetrakis(acetonitrile)copper(I) trifluoromethanesulfonate (58452-28-1) → (N,N'-bis-2,6-diisopropylphenyl-2,4-dimethyl-1,5-diketamide)Cu(acetonitrile) (410527-15-0)

Guidance literature:

N,N′-bis(2,6-diisopropylphenyl)pentane-2,4-diimine; With n-butyllithium; In tetrahydrofuran; hexane; at 20 ℃; for 3h; Inert atmosphere;

tetrakis(acetonitrile)copper(I) trifluoromethanesulfonate; In tetrahydrofuran; hexane; at 20 ℃; for 0.166667h; Inert atmosphere;

DOI:10.1021/jacs.0c07137

Reference yield: 65.0%

[copper(O2CCH3)(N(2,6-diisopropylphenyl)C(CH3))2CH] (896420-80-7) + acetonitrile (75-05-8,26809-02-9) + sodium disulfide (22868-13-9) → (N,N'-bis-2,6-diisopropylphenyl-2,4-dimethyl-1,5-diketamide)Cu(acetonitrile) (410527-15-0)

Guidance literature:

In acetonitrile; addn. of suspn. of sodium disulfide to soln. of copper compd. in CH3CN, stirring for 30 min under Ar; filtration, drying, IR and MS;

DOI:10.1039/b808678h

Reference yield:

tetrakis(acetonitrile)copper(I) trifluoromethanesulfonate (58452-28-1) + (2-((2,6-diisopropylphenyl)amino)-4-((2,6-diisopropylphenyl)imino)-pent-2-ene) lithium salt → (N,N'-bis-2,6-diisopropylphenyl-2,4-dimethyl-1,5-diketamide)Cu(acetonitrile) (410527-15-0)

Guidance literature:

In not given; in THF or toluene;

DOI:10.1021/ja017820b

upstream raw materials:

tetrakis(acetonitrile)copper(I) trifluoromethanesulfonate

[copper(O₂CCH₃)(N(2,6-diisopropylphenyl)C(CH₃))2CH]

acetonitrile

sodium disulfide

Downstream raw materials:

(N,N'-bis-2,6-diisopropylphenyl-2,4-dimethyl-1,5-diketamide)Cu(O₂)

Cu⁽¹⁸⁾O₂(CH(C(CH₃)NC₆H₃(CH(CH₃)2)2)2)

((C₆H₃(CH(CH₃)2)2NCCH₃)2CHCu)2NCC₆H₄CN

(C₆H₃(CH(CH₃)2)2NCCH₃)2CHCu(NCC₆H₅)

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