dimethyl (3-(2,5,8,11-tetraoxatridecan-13-yloxy)phenyl)phosphonite borane

Base Information

Chemical Name:dimethyl (3-(2,5,8,11-tetraoxatridecan-13-yloxy)phenyl)phosphonite borane
CAS No.:1337878-57-5
Molecular Formula:C₁₇H₃₂BO₇P
Molecular Weight:390.222
Hs Code.:

Synonyms:dimethyl (3-(2,5,8,11-tetraoxatridecan-13-yloxy)phenyl)phosphonite borane

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Chemical Property of dimethyl (3-(2,5,8,11-tetraoxatridecan-13-yloxy)phenyl)phosphonite borane

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Technology Process of dimethyl (3-(2,5,8,11-tetraoxatridecan-13-yloxy)phenyl)phosphonite borane

There total 1 articles about dimethyl (3-(2,5,8,11-tetraoxatridecan-13-yloxy)phenyl)phosphonite borane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1337529-86-8
dimethyl (3-(2,5,8,11-tetraoxatridecan-13-yloxy)phenyl)phosphonite

: 1337878-57-5
dimethyl (3-(2,5,8,11-tetraoxatridecan-13-yloxy)phenyl)phosphonite borane

Guidance literature:: With dimethylsulfide borane complex; In diethyl ether; at 20 ℃; for 15h;
DOI:10.1021/ol2020175

Reference yield: 46.0%

: 1337878-57-5
dimethyl (3-(2,5,8,11-tetraoxatridecan-13-yloxy)phenyl)phosphonite borane

: 1337529-86-8
dimethyl (3-(2,5,8,11-tetraoxatridecan-13-yloxy)phenyl)phosphonite

Guidance literature:: With 1,4-diaza-bicyclo[2.2.2]octane; In benzene; at 50 ℃; for 22h;
DOI:10.1021/ol2020175

Reference yield:

: 1337878-57-5
dimethyl (3-(2,5,8,11-tetraoxatridecan-13-yloxy)phenyl)phosphonite borane

: C₆₁H₉₀N₁₁O₁₉P

Guidance literature:: Multi-step reaction with 2 steps

1: 1,4-diaza-bicyclo[2.2.2]octane / benzene / 22 h / 50 °C

2: dimethyl sulfoxide / 4 h / 20 °C / pH 8.2 / tris/HCl buffer

With 1,4-diaza-bicyclo[2.2.2]octane; In dimethyl sulfoxide; benzene; 2: Staudinger reaction;
DOI:10.1021/ol2020175