methyl 2,3-di-O-p-methoxybenzyl-4-acetylthio-6-deoxy-α-D-galactopyranoside

Base Information

Chemical Name:methyl 2,3-di-O-p-methoxybenzyl-4-acetylthio-6-deoxy-α-D-galactopyranoside
CAS No.:1404060-82-7
Molecular Formula:C₂₅H₃₂O₇S
Molecular Weight:476.591
Hs Code.:

Synonyms:methyl 2,3-di-O-p-methoxybenzyl-4-acetylthio-6-deoxy-α-D-galactopyranoside

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of methyl 2,3-di-O-p-methoxybenzyl-4-acetylthio-6-deoxy-α-D-galactopyranoside

Chemical Property:

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Technology Process of methyl 2,3-di-O-p-methoxybenzyl-4-acetylthio-6-deoxy-α-D-galactopyranoside

There total 4 articles about methyl 2,3-di-O-p-methoxybenzyl-4-acetylthio-6-deoxy-α-D-galactopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₂₄H₂₉F₃O₉S

: 10387-40-3
potassium thioacetate

: 1404060-82-7
methyl 2,3-di-O-p-methoxybenzyl-4-acetylthio-6-deoxy-α-D-galactopyranoside

Guidance literature:: In N,N-dimethyl-formamide; at 20 - 90 ℃; for 2h;
DOI:10.1016/j.tet.2012.09.037

Reference yield:

: 922733-50-4
methyl 2,3-di-O-p-methoxybenzyl-6-deoxy-α-D-glucopyranoside

: 1404060-82-7
methyl 2,3-di-O-p-methoxybenzyl-4-acetylthio-6-deoxy-α-D-galactopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine / dichloromethane / 2 h / -30 - 20 °C

2: N,N-dimethyl-formamide / 2 h / 20 - 90 °C

With pyridine; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/j.tet.2012.09.037

Reference yield:

: C₃₀H₃₆O₈

: 1404060-82-7
methyl 2,3-di-O-p-methoxybenzyl-4-acetylthio-6-deoxy-α-D-galactopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: lithium aluminium tetrahydride / tetrahydrofuran / 20 °C / Reflux

2: pyridine / dichloromethane / 2 h / -30 - 20 °C

3: N,N-dimethyl-formamide / 2 h / 20 - 90 °C

With pyridine; lithium aluminium tetrahydride; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/j.tet.2012.09.037