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C2HF3O2*C23H25FN2O

Base Information
  • Chemical Name:C2HF3O2*C23H25FN2O
  • CAS No.:1283086-04-3
  • Molecular Formula:C2HF3O2*C23H25FN2O
  • Molecular Weight:478.487
  • Hs Code.:
C<sub>2</sub>HF<sub>3</sub>O<sub>2</sub>*C<sub>23</sub>H<sub>25</sub>FN<sub>2</sub>O

Synonyms:C2HF3O2*C23H25FN2O

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Chemical Property of C2HF3O2*C23H25FN2O
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Technology Process of C2HF3O2*C23H25FN2O

There total 4 articles about C2HF3O2*C23H25FN2O which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
7-methyl-3,4,5,10-tetrahydro-1H-2,5-methanoazepino[3,4-b]indole; With sodium hydride; In N,N-dimethyl-formamide; at 20 ℃; for 0.166667h;
p-fluoro-α-methylstyrene oxide; In N,N-dimethyl-formamide; at 20 ℃;
trifluoroacetic acid;
Guidance literature:
Multi-step reaction with 4 steps
1.1: acetic acid / 24 h / 90 °C
2.1: lithium aluminium tetrahydride / tetrahydrofuran / Inert atmosphere; Reflux
3.1: trifluoroacetic acid / ethanol / 3 h / Reflux
3.2: 2 h / Reflux
4.1: sodium hydride / N,N-dimethyl-formamide / 0.17 h / 20 °C
4.2: 20 °C
With lithium aluminium tetrahydride; sodium hydride; acetic acid; trifluoroacetic acid; In tetrahydrofuran; ethanol; N,N-dimethyl-formamide; 3.1: Pictet-Spengler Cyclisation / 3.2: Pictet-Spengler Cyclisation;
Guidance literature:
Multi-step reaction with 3 steps
1.1: lithium aluminium tetrahydride / tetrahydrofuran / Inert atmosphere; Reflux
2.1: trifluoroacetic acid / ethanol / 3 h / Reflux
2.2: 2 h / Reflux
3.1: sodium hydride / N,N-dimethyl-formamide / 0.17 h / 20 °C
3.2: 20 °C
With lithium aluminium tetrahydride; sodium hydride; trifluoroacetic acid; In tetrahydrofuran; ethanol; N,N-dimethyl-formamide; 2.1: Pictet-Spengler Cyclisation / 2.2: Pictet-Spengler Cyclisation;
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