dibenzyl 2-(5-methylselenophen-2-yl)-6,7-methylenedioxyquinolin-4-yl phosphate

Base Information

Chemical Name:dibenzyl 2-(5-methylselenophen-2-yl)-6,7-methylenedioxyquinolin-4-yl phosphate
CAS No.:1350903-43-3
Molecular Formula:C₂₉H₂₄NO₆PSe
Molecular Weight:592.446
Hs Code.:

Synonyms:dibenzyl 2-(5-methylselenophen-2-yl)-6,7-methylenedioxyquinolin-4-yl phosphate

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Chemical Property of dibenzyl 2-(5-methylselenophen-2-yl)-6,7-methylenedioxyquinolin-4-yl phosphate

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Technology Process of dibenzyl 2-(5-methylselenophen-2-yl)-6,7-methylenedioxyquinolin-4-yl phosphate

There total 4 articles about dibenzyl 2-(5-methylselenophen-2-yl)-6,7-methylenedioxyquinolin-4-yl phosphate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.9%

: 990-91-0
dibenzyl [[bis(benzyloxy)phosphoryl]oxy]phosphonate

: 1350903-16-0
2-(5-methylselenophen-2-yl)-6,7-methylenedioxyquinolin-4(1H)-one

: 1350903-43-3
dibenzyl 2-(5-methylselenophen-2-yl)-6,7-methylenedioxyquinolin-4-yl phosphate

Guidance literature:: With sodium hydride; In tetrahydrofuran; for 0.333333h;
DOI:10.1016/j.ejmech.2011.10.017

Reference yield:

: 1350903-35-3
N-(6-acetylbenzo[d][1,3]dioxol-5-yl)-5-methylselenophene-2-carboxamide

: 1350903-43-3
dibenzyl 2-(5-methylselenophen-2-yl)-6,7-methylenedioxyquinolin-4-yl phosphate

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium hydroxide / 1,4-dioxane / 16 h / Reflux

1.2: 0.5 h

2.1: sodium hydride / tetrahydrofuran / 0.33 h

With sodium hydride; sodium hydroxide; In tetrahydrofuran; 1,4-dioxane;
DOI:10.1016/j.ejmech.2011.10.017

Reference yield:

: 22988-84-7
5-methylselenophene-2-carboxylic acid

: 1350903-43-3
dibenzyl 2-(5-methylselenophen-2-yl)-6,7-methylenedioxyquinolin-4-yl phosphate

Guidance literature:: Multi-step reaction with 4 steps

1.1: thionyl chloride; N,N-dimethyl-formamide / toluene / 16 h

2.1: triethylamine / toluene / 48 h / 20 °C

3.1: sodium hydroxide / 1,4-dioxane / 16 h / Reflux

3.2: 0.5 h

4.1: sodium hydride / tetrahydrofuran / 0.33 h

With thionyl chloride; sodium hydride; triethylamine; N,N-dimethyl-formamide; sodium hydroxide; In tetrahydrofuran; 1,4-dioxane; toluene;
DOI:10.1016/j.ejmech.2011.10.017