trimethyl (2R,3R,4R,5S)-5-(4-chlorophenyl)pyrrolidine-2,3,4-tricarboxylate

Base Information

Chemical Name:trimethyl (2R,3R,4R,5S)-5-(4-chlorophenyl)pyrrolidine-2,3,4-tricarboxylate
CAS No.:1166397-85-8
Molecular Formula:C₁₆H₁₈ClNO₆
Molecular Weight:355.775
Hs Code.:

Synonyms:trimethyl (2R,3R,4R,5S)-5-(4-chlorophenyl)pyrrolidine-2,3,4-tricarboxylate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of trimethyl (2R,3R,4R,5S)-5-(4-chlorophenyl)pyrrolidine-2,3,4-tricarboxylate

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Technology Process of trimethyl (2R,3R,4R,5S)-5-(4-chlorophenyl)pyrrolidine-2,3,4-tricarboxylate

There total 2 articles about trimethyl (2R,3R,4R,5S)-5-(4-chlorophenyl)pyrrolidine-2,3,4-tricarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 76862-09-4
methyl N-(4-chlorobenzylidene)glycinate

: 624-49-7
dimethylfumarate

: trimethyl (2S,3S,4S,5R)-5-(4-chlorophenyl)pyrrolidine-2,3,4-tricarboxylate

: 1166397-85-8
trimethyl (2R,3R,4R,5S)-5-(4-chlorophenyl)pyrrolidine-2,3,4-tricarboxylate

: trimethyl 5-(4-chlorophenyl)pyrrolidine-2,3,4-tricarboxylate

Guidance literature:: With 3-{(S)-1-[(S)-2-(diphenylphosphino)ferrocenyl]ethyl}-2-(phenylthio)indole; silver(I) acetate; triethylamine; In diethyl ether; at -40 ℃; for 18h; optical yield given as %ee; enantioselective reaction; Inert atmosphere;
DOI:10.1016/j.tetasy.2012.02.017

Reference yield:

: 76862-09-4
methyl N-(4-chlorobenzylidene)glycinate

: 624-49-7
dimethylfumarate

: trimethyl (2S,3S,4S,5R)-5-(4-chlorophenyl)pyrrolidine-2,3,4-tricarboxylate

: 1166397-85-8
trimethyl (2R,3R,4R,5S)-5-(4-chlorophenyl)pyrrolidine-2,3,4-tricarboxylate

Guidance literature:: With C₄₉H₃₉FeNO₂P₂; silver(I) acetate; triethylamine; In diethyl ether; at -25 ℃; for 15h; optical yield given as %ee; enantioselective reaction; Inert atmosphere;
DOI:10.1016/j.tetasy.2009.02.058