(E)-(2S,8R,15R)-15-Isobutyl-8-(4-methoxy-benzyl)-2-((E)-(R)-1-methyl-3-phenyl-allyl)-1-oxa-7,10-diaza-cyclohexadec-4-ene-6,9,13,16-tetraone

Base Information

• Chemical Name: (E)-(2S,8R,15R)-15-Isobutyl-8-(4-methoxy-benzyl)-2-((E)-(R)-1-methyl-3-phenyl-allyl)-1-oxa-7,10-diaza-cyclohexadec-4-ene-6,9,13,16-tetraone
• CAS No.: 302600-53-9
• Molecular Formula: C₃₅H₄₄N₂O₆
• Molecular Weight: 588.744

Synonyms:(E)-(2S,8R,15R)-15-Isobutyl-8-(4-methoxy-benzyl)-2-((E)-(R)-1-methyl-3-phenyl-allyl)-1-oxa-7,10-diaza-cyclohexadec-4-ene-6,9,13,16-tetraone

Chemical Property of (E)-(2S,8R,15R)-15-Isobutyl-8-(4-methoxy-benzyl)-2-((E)-(R)-1-methyl-3-phenyl-allyl)-1-oxa-7,10-diaza-cyclohexadec-4-ene-6,9,13,16-tetraone

Chemical Property:

Purity/Quality:

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Technology Process of (E)-(2S,8R,15R)-15-Isobutyl-8-(4-methoxy-benzyl)-2-((E)-(R)-1-methyl-3-phenyl-allyl)-1-oxa-7,10-diaza-cyclohexadec-4-ene-6,9,13,16-tetraone

There total 1 articles about (E)-(2S,8R,15R)-15-Isobutyl-8-(4-methoxy-benzyl)-2-((E)-(R)-1-methyl-3-phenyl-allyl)-1-oxa-7,10-diaza-cyclohexadec-4-ene-6,9,13,16-tetraone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(R)-6-Amino-2-isobutyl-4-oxo-hexanoic acid (E)-(1S,2R)-1-{(E)-3-[(R)-1-carboxy-2-(4-methoxy-phenyl)-ethylcarbamoyl]-allyl}-2-methyl-4-phenyl-but-3-enyl ester; hydrochloride → (E)-(2S,8R,15R)-15-Isobutyl-8-(4-methoxy-benzyl)-2-((E)-(R)-1-methyl-3-phenyl-allyl)-1-oxa-7,10-diaza-cyclohexadec-4-ene-6,9,13,16-tetraone (302600-53-9)

Guidance literature:

With diphenyl-phosphinic acid; sodium hydrogencarbonate; In N,N-dimethyl-formamide; at 5 ℃;

DOI:10.1016/S0960-894X(00)00356-5

Reference yield: 66.0%

(E)-(2S,8R,15R)-15-Isobutyl-8-(4-methoxy-benzyl)-2-((E)-(R)-1-methyl-3-phenyl-allyl)-1-oxa-7,10-diaza-cyclohexadec-4-ene-6,9,13,16-tetraone (302600-53-9) → (E)-(2S,8R,15R)-15-Isobutyl-8-(4-methoxy-benzyl)-2-[(S)-1-((2R,3R)-3-phenyl-oxiranyl)-ethyl]-1-oxa-7,10-diaza-cyclohexadec-4-ene-6,9,13,16-tetraone + (E)-(2S,8R,15R)-15-Isobutyl-8-(4-methoxy-benzyl)-2-[(S)-1-((2S,3S)-3-phenyl-oxiranyl)-ethyl]-1-oxa-7,10-diaza-cyclohexadec-4-ene-6,9,13,16-tetraone

Guidance literature:

With 3,3-dimethyldioxirane; In dichloromethane; acetone; at -10 ℃; for 3h;

DOI:10.1016/S0040-4020(01)00339-8

Reference yield: 66.0%

(E)-(2S,8R,15R)-15-Isobutyl-8-(4-methoxy-benzyl)-2-((E)-(R)-1-methyl-3-phenyl-allyl)-1-oxa-7,10-diaza-cyclohexadec-4-ene-6,9,13,16-tetraone (302600-53-9) → (E)-(2S,8R,15R)-15-Isobutyl-8-(4-methoxy-benzyl)-2-[(S)-1-((2R,3R)-3-phenyl-oxiranyl)-ethyl]-1-oxa-7,10-diaza-cyclohexadec-4-ene-6,9,13,16-tetraone

Guidance literature:

With 3,3-dimethyldioxirane; In dichloromethane;

DOI:10.1016/S0960-894X(00)00356-5

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