methyl O,N-dimethyl-L-tyr-L-alaninate

Base Information

Chemical Name:methyl O,N-dimethyl-L-tyr-L-alaninate
CAS No.:91474-98-5
Molecular Formula:C₁₅H₂₂N₂O₄
Molecular Weight:294.351
Hs Code.:

Synonyms:methyl O,N-dimethyl-L-tyr-L-alaninate

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Chemical Property of methyl O,N-dimethyl-L-tyr-L-alaninate

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Technology Process of methyl O,N-dimethyl-L-tyr-L-alaninate

There total 6 articles about methyl O,N-dimethyl-L-tyr-L-alaninate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 91474-97-4
methyl O,N-dimethyl-N-boc-L-tyr-L-alaninate

: 91474-98-5
methyl O,N-dimethyl-L-tyr-L-alaninate

Guidance literature:: With trifluoroacetic acid; In dichloromethane; at 25 ℃; for 0.5h;
DOI:10.1021/jo00238a005

Reference yield:

: 115441-65-1
methyl N-Cbz-N,O-dimethyl-L-tyrosyl-L-alaninate

: 91474-98-5
methyl O,N-dimethyl-L-tyr-L-alaninate

Guidance literature:: With hydrogenchloride; hydrogen; palladium on activated charcoal; In methanol; at 20 ℃; for 2h;
DOI:10.1021/jo030293p

Reference yield:

: 86099-14-1
(2S)-3-(4-hydroxyphenyl)-2-(methyl{[(phenylmethyl)oxy]carbonyl}amino)propanoic acid

: 91474-98-5
methyl O,N-dimethyl-L-tyr-L-alaninate

Guidance literature:: Multi-step reaction with 3 steps

1: 71 percent / HOBt; Et₃N; EDC / CH₂Cl₂ / 16 h / 20 °C

2: 100 percent / methanol; diethyl ether

3: H₂; hydrochloric acid / Pd/C / methanol / 2 h / 20 °C

With hydrogenchloride; hydrogen; benzotriazol-1-ol; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; triethylamine; palladium on activated charcoal; In methanol; diethyl ether; dichloromethane;
DOI:10.1021/jo030293p