2-methoxy-3-nitrophenyl N,N-diethylcarbamate

Base Information

Chemical Name:2-methoxy-3-nitrophenyl N,N-diethylcarbamate
CAS No.:858647-47-9
Molecular Formula:C₁₂H₁₆N₂O₅
Molecular Weight:268.269
Hs Code.:

Synonyms:2-methoxy-3-nitrophenyl N,N-diethylcarbamate

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Chemical Property of 2-methoxy-3-nitrophenyl N,N-diethylcarbamate

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Technology Process of 2-methoxy-3-nitrophenyl N,N-diethylcarbamate

There total 3 articles about 2-methoxy-3-nitrophenyl N,N-diethylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 858647-49-1
2-methoxy-3-nitro-6-(trimethylsilyl)phenyl N,N-diethylcarbamate

: 858647-47-9
2-methoxy-3-nitrophenyl N,N-diethylcarbamate

Guidance literature:: With cesium fluoride; In N,N-dimethyl-formamide; for 0.666667h; Heating;
DOI:10.1021/ol0506563

Reference yield: 52.0%

: 85630-19-9
N,N-diethyl-1-carbamyloxy-2-methoxybenzene

: 2-methoxy-5-nitrophenyl N,N-diethylcarbamate

: 858647-47-9
2-methoxy-3-nitrophenyl N,N-diethylcarbamate

Guidance literature:: With nitric acid; acetic anhydride; at 0 ℃; for 1h;
DOI:10.1021/ol0506563

Reference yield:

: O-(2-methoxy-6-trimethylsilyl)phenyl N,N-diethylcarbamate

: 858647-47-9
2-methoxy-3-nitrophenyl N,N-diethylcarbamate

Guidance literature:: Multi-step reaction with 2 steps

1: 76 percent / aq. HNO₃; Ac₂O / 1 h / 0 °C

2: 90 percent / CsF / dimethylformamide / 0.67 h / Heating

With nitric acid; acetic anhydride; cesium fluoride; In N,N-dimethyl-formamide;
DOI:10.1021/ol0506563