2,2′-Bis(4-methylbenzolsulfonylamido)-diphenyldisulfid

Base Information

Chemical Name:2,2′-Bis(4-methylbenzolsulfonylamido)-diphenyldisulfid
CAS No.:3982-42-1
Molecular Formula:C26H24N2O4S4
Molecular Weight:556.752
Hs Code.:
Mol file:3982-42-1.mol

Synonyms:o-Tosylamidophenyl-Disulfid;Di-(o-tosylaminophenyl)disulfid;N,N'-(Dithiobis(2,1-phenylene))bis(4-methylbenzenesulfonamide);2,2'-Bis-p-toluolsulfonylamino-diphenyldisulfid;bis-[2-(toluene-4-sulfonylamino)-phenyl]-disulfane;bis<2-(p-toluenesulfonamido)phenyl> disulfide;

Suppliers and Price of 2,2′-Bis(4-methylbenzolsulfonylamido)-diphenyldisulfid

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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Total 1 raw suppliers

Chemical Property of 2,2′-Bis(4-methylbenzolsulfonylamido)-diphenyldisulfid

Chemical Property:

Boiling Point:685.2°Cat760mmHg
Flash Point:368.2°C
PSA：159.70000
Density:1.46g/cm³
LogP:9.01200

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 2,2′-Bis(4-methylbenzolsulfonylamido)-diphenyldisulfid

There total 5 articles about 2,2′-Bis(4-methylbenzolsulfonylamido)-diphenyldisulfid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 98-59-9
p-toluenesulfonyl chloride

: 1141-88-4
2-Aminophenyl disulfide

: 3982-42-1
N,N'-(disulfanediylbis(2,1-phenylene))bis(4-methylbenzenesulfonamide)

Guidance literature:: With pyridine; at 20 ℃;
DOI:10.1016/j.bioorg.2016.07.002

Reference yield: 61.0%

: 104-15-4
toluene-4-sulfonic acid

: 1141-88-4
2-Aminophenyl disulfide

: 3982-42-1
N,N'-(disulfanediylbis(2,1-phenylene))bis(4-methylbenzenesulfonamide)

Guidance literature:: With 4-methyl-morpholine; diisopropyl-carbodiimide; In tetrahydrofuran; for 20h;

Reference yield:

: 137-07-5
2-amino-benzenethiol

: 3982-42-1
N,N'-(disulfanediylbis(2,1-phenylene))bis(4-methylbenzenesulfonamide)

Guidance literature:: Multi-step reaction with 2 steps

1: periodic acid; sodium hydrogensulfite / water / 3 h / 20 °C

2: pyridine / 20 °C

With pyridine; sodium hydrogensulfite; periodic acid; In water;
DOI:10.1016/j.bioorg.2016.07.002