(+/-)-Benzyl N-(benzyloxycarbonyl)-α-vinylvalinate

Base Information

Chemical Name:(+/-)-Benzyl N-(benzyloxycarbonyl)-α-vinylvalinate
CAS No.:157794-60-0
Molecular Formula:C₂₂H₂₅NO₄
Molecular Weight:367.445
Hs Code.:

Synonyms:(+/-)-Benzyl N-(benzyloxycarbonyl)-α-vinylvalinate

Suppliers and Price of (+/-)-Benzyl N-(benzyloxycarbonyl)-α-vinylvalinate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of (+/-)-Benzyl N-(benzyloxycarbonyl)-α-vinylvalinate

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of (+/-)-Benzyl N-(benzyloxycarbonyl)-α-vinylvalinate

There total 1 articles about (+/-)-Benzyl N-(benzyloxycarbonyl)-α-vinylvalinate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 152884-32-7
α-Vinylvaline

: 501-53-1,94274-21-2
benzyl chloroformate

: 157794-60-0
(+/-)-Benzyl N-(benzyloxycarbonyl)-α-vinylvalinate

Guidance literature:: With dmap; triethylamine; In dimethyl sulfoxide; for 2h; Heating;
DOI:10.1021/jo00097a064

Reference yield:

: 157794-60-0
(+/-)-Benzyl N-(benzyloxycarbonyl)-α-vinylvalinate

: ((3R,4R)-4-Hydroxy-3-isopropyl-2-oxo-tetrahydro-furan-3-yl)-carbamic acid benzyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: OsO₄, NMO

2: NaH / dimethylformamide

With osmium(VIII) oxide; N-methyl-2-indolinone; sodium hydride; In N,N-dimethyl-formamide;
DOI:10.1021/jo00122a002