C₂F₃O₂^(1-)C₂HF₃O₂C₃₀H₃₁N₂O₄⁽¹⁺⁾

Base Information

Chemical Name:C₂F₃O₂^(1-)*C₂HF₃O₂*C₃₀H₃₁N₂O₄⁽¹⁺⁾
CAS No.:1235871-18-7
Molecular Formula:C₂F₃O₂*C₂HF₃O₂*C₃₀H₃₁N₂O₄
Molecular Weight:710.627
Hs Code.:

C<sub>2</sub>F<sub>3</sub>O<sub>2</sub><sup>(1-)</sup>*C<sub>2</sub>HF<sub>3</sub>O<sub>2</sub>*C<sub>30</sub>H<sub>31</sub>N<sub>2</sub>O<sub>4</sub><sup>(1+)</sup>

Synonyms:C₂F₃O₂^(1-)*C₂HF₃O₂*C₃₀H₃₁N₂O₄⁽¹⁺⁾

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Chemical Property of C₂F₃O₂^(1-)*C₂HF₃O₂*C₃₀H₃₁N₂O₄⁽¹⁺⁾

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Technology Process of C₂F₃O₂^(1-)*C₂HF₃O₂*C₃₀H₃₁N₂O₄⁽¹⁺⁾

There total 7 articles about C₂F₃O₂^(1-)*C₂HF₃O₂*C₃₀H₃₁N₂O₄⁽¹⁺⁾ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 52.0%

: 1235871-90-5
C₃₀H₃₀N₂O₅

: 76-05-1
trifluoroacetic acid

: 1235871-18-7
C₂F₃O₂^(1-)*C₂HF₃O₂*C₃₀H₃₁N₂O₄⁽¹⁺⁾

Guidance literature:: With lithium aluminium tetrahydride; In tetrahydrofuran;

Reference yield:

: 1235871-87-0
C₂₀H₂₂N₂O₂

: 1235871-18-7
C₂F₃O₂^(1-)*C₂HF₃O₂*C₃₀H₃₁N₂O₄⁽¹⁺⁾

Guidance literature:: Multi-step reaction with 4 steps

1.1: triethylamine / dmap / dichloromethane / 20 °C

2.1: sodium hydride / water; N,N-dimethyl-formamide / 0.17 h

2.2: 19 h / 20 °C

3.1: tris-(o-tolyl)phosphine; silver carbonate / palladium diacetate / Inert atmosphere

4.1: lithium aluminium tetrahydride / tetrahydrofuran

With lithium aluminium tetrahydride; sodium hydride; triethylamine; tris-(o-tolyl)phosphine; silver carbonate; dmap; palladium diacetate; In tetrahydrofuran; dichloromethane; water; N,N-dimethyl-formamide;

Reference yield:

: 1235871-86-9
C₂₀H₂₀N₂O₄

: 1235871-18-7
C₂F₃O₂^(1-)*C₂HF₃O₂*C₃₀H₃₁N₂O₄⁽¹⁺⁾

Guidance literature:: Multi-step reaction with 5 steps

1.1: hydrazine hydrate / palladium 10% on activated carbon / ethanol / 3 h / 80 °C / Inert atmosphere

2.1: triethylamine / dmap / dichloromethane / 20 °C

3.1: sodium hydride / water; N,N-dimethyl-formamide / 0.17 h

3.2: 19 h / 20 °C

4.1: tris-(o-tolyl)phosphine; silver carbonate / palladium diacetate / Inert atmosphere

5.1: lithium aluminium tetrahydride / tetrahydrofuran

With lithium aluminium tetrahydride; sodium hydride; hydrazine hydrate; triethylamine; tris-(o-tolyl)phosphine; silver carbonate; dmap; palladium 10% on activated carbon; palladium diacetate; In tetrahydrofuran; ethanol; dichloromethane; water; N,N-dimethyl-formamide;