17β-hydroxy-4β,5-cyclopropano-5(10a)-homo-19-nor-5β-androst-1(10)-en-3-one 17-benzoate

Base Information

Chemical Name:17β-hydroxy-4β,5-cyclopropano-5(10a)-homo-19-nor-5β-androst-1(10)-en-3-one 17-benzoate
CAS No.:123715-74-2
Molecular Formula:C₂₇H₃₂O₃
Molecular Weight:404.549
Hs Code.:

Synonyms:17β-hydroxy-4β,5-cyclopropano-5(10a)-homo-19-nor-5β-androst-1(10)-en-3-one 17-benzoate

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Chemical Property of 17β-hydroxy-4β,5-cyclopropano-5(10a)-homo-19-nor-5β-androst-1(10)-en-3-one 17-benzoate

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Technology Process of 17β-hydroxy-4β,5-cyclopropano-5(10a)-homo-19-nor-5β-androst-1(10)-en-3-one 17-benzoate

There total 3 articles about 17β-hydroxy-4β,5-cyclopropano-5(10a)-homo-19-nor-5β-androst-1(10)-en-3-one 17-benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 123715-69-5,123806-54-2
4β,5-cyclopropano-5(10a)-homo-19-nor-5β-androst-1(10)-ene-3β,17β-diol 17-benzoate

: 123715-74-2
17β-hydroxy-4β,5-cyclopropano-5(10a)-homo-19-nor-5β-androst-1(10)-en-3-one 17-benzoate

Guidance literature:: With jones' reagent; In acetone; for 0.116667h; Ambient temperature;

Reference yield: 60.0%

: 123715-69-5,123806-54-2
4β,5-cyclopropano-5(10a)-homo-19-nor-5β-androst-1(10)-ene-3α,17β-diol 17-benzoate

: 123715-74-2
17β-hydroxy-4β,5-cyclopropano-5(10a)-homo-19-nor-5β-androst-1(10)-en-3-one 17-benzoate

Guidance literature:: With jones' reagent; In acetone; for 0.116667h; Ambient temperature;

Reference yield:

: 123715-70-8
4β,5-cyclopropano-5(10a)-homo-19-nor-5β-adrosta-1(10)-ene-3α,17β-diol 3-acetate 17-benzoate

: 123715-74-2
17β-hydroxy-4β,5-cyclopropano-5(10a)-homo-19-nor-5β-androst-1(10)-en-3-one 17-benzoate

Guidance literature:: Multi-step reaction with 2 steps

1: 64 percent / K₂CO₃ / H₂O; methanol / 4 h / 35 °C

2: 60 percent / Jones' reagent / acetone / 0.12 h / Ambient temperature

With jones' reagent; potassium carbonate; In methanol; water; acetone;