2,3,9,10-tetramethoxy-5-hydroxy-6α-(3,4-dimethoxyphenyl)-7-(3,4-dimethoxybenzoyl)-5,6,7,15-tetrahydro-6-oxoniabenzanthracene

Base Information

• Chemical Name: 2,3,9,10-tetramethoxy-5-hydroxy-6α-(3,4-dimethoxyphenyl)-7-(3,4-dimethoxybenzoyl)-5,6,7,15-tetrahydro-6-oxoniabenz
• Molecular Formula: C₃₈H₃₈O₁₁
• Molecular Weight: 670.713

Synonyms:2,3,9,10-tetramethoxy-5-hydroxy-6α-(3,4-dimethoxyphenyl)-7-(3,4-dimethoxybenzoyl)-5,6,7,15-tetrahydro-6-oxoniabenzanthracene

Chemical Property of 2,3,9,10-tetramethoxy-5-hydroxy-6α-(3,4-dimethoxyphenyl)-7-(3,4-dimethoxybenzoyl)-5,6,7,15-tetrahydro-6-oxoniabenz

Chemical Property:

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There total 2 articles about 2,3,9,10-tetramethoxy-5-hydroxy-6α-(3,4-dimethoxyphenyl)-7-(3,4-dimethoxybenzoyl)-5,6,7,15-tetrahydro-6-oxoniabenzanthracene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

1-(3,4-dimethoxybenzoyl)-1-(2-formyl-4,5-dimethoxyphenyl)-2-<2-(3,4-dimethoxyphenyl)-4,5-dimethoxyphenyl>ethylene (135330-73-3) → 2,3,9,10-tetramethoxy-5-hydroxy-6α-(3,4-dimethoxyphenyl)-7-(3,4-dimethoxybenzoyl)-5,6,7,15-tetrahydro-6-oxoniabenzanthracene (135330-74-4)

Guidance literature:

With potassium hydroxide; In 1,4-dioxane; for 0.5h;

DOI:10.1007/BF00476745

Reference yield: 85.0%

1-<α-(3,4-dimethoxybenzoyl)(2-ormyl-4,5-dimethoxybenzyl)>-3-(3,4-dimethoxyphenyl)-6,7-dimethoxyisochromene (125416-96-8) → 2,3,9,10-tetramethoxy-5-hydroxy-6α-(3,4-dimethoxyphenyl)-7-(3,4-dimethoxybenzoyl)-5,6,7,15-tetrahydro-6-oxoniabenzanthracene (135330-74-4)

Guidance literature:

With potassium hydroxide; In 1,4-dioxane; for 0.333333h;

DOI:10.1007/BF00476745

Reference yield: 55.0%

2,3,9,10-tetramethoxy-5-hydroxy-6α-(3,4-dimethoxyphenyl)-7-(3,4-dimethoxybenzoyl)-5,6,7,15-tetrahydro-6-oxoniabenzanthracene (135330-74-4) → 2-(2-formyl-4,5-dimethoxyphenyl)-3-(3,4-dimethoxyphenyl)-6,7-dimethoxynaphthalene (135330-80-2) + 1-(3,4-dimethoxybenzoyl)-2-(3,4-dimethoxyphenyl)-3-(2-formyl-4,5-dimethoxyphenyl)-6,7-dimethoxynaphthalene (135330-76-6) + Veratric acid (93-07-2)

Guidance literature:

With acetic acid; Heating;

DOI:10.1007/BF00476745

upstream raw materials:

1-<α-(3,4-dimethoxybenzoyl)(2-ormyl-4,5-dimethoxybenzyl)>-3-(3,4-dimethoxyphenyl)-6,7-dimethoxyisochromene

1-(3,4-dimethoxybenzoyl)-1-(2-formyl-4,5-dimethoxyphenyl)-2-<2-(3,4-dimethoxyphenyl)-4,5-dimethoxyphenyl>ethylene

Downstream raw materials:

2-(3,4-dimethoxyphenyl)-3-(2-carboxy-4,5-dimethoxyphenyl)-6,7-dimethoxynaphthalene

1-(3,4-dimethoxybenzoyl)-2-(3,4-dimethoxyphenyl)-3-(2-formyl-4,5-dimethoxyphenyl)-6,7-dimethoxynaphthalene

2-(2-formyl-4,5-dimethoxyphenyl)-3-(3,4-dimethoxyphenyl)-6,7-dimethoxynaphthalene

Veratric acid

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