(2R,3S)-5-Benzenesulfonyl-3-methyl-2-((S)-1-methyl-allyl)-tetrahydro-furan

Base Information

Chemical Name:(2R,3S)-5-Benzenesulfonyl-3-methyl-2-((S)-1-methyl-allyl)-tetrahydro-furan
CAS No.:213262-40-9
Molecular Formula:C₁₅H₂₀O₃S
Molecular Weight:280.388
Hs Code.:

Synonyms:(2R,3S)-5-Benzenesulfonyl-3-methyl-2-((S)-1-methyl-allyl)-tetrahydro-furan

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (2R,3S)-5-Benzenesulfonyl-3-methyl-2-((S)-1-methyl-allyl)-tetrahydro-furan

Chemical Property:

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Technology Process of (2R,3S)-5-Benzenesulfonyl-3-methyl-2-((S)-1-methyl-allyl)-tetrahydro-furan

There total 5 articles about (2R,3S)-5-Benzenesulfonyl-3-methyl-2-((S)-1-methyl-allyl)-tetrahydro-furan which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 618-41-7
Benzenesulfinic acid

: 213262-39-6
(1'S,2R,4S,5R)-Tetrahydro-4-methyl-5-(1'-methylprop-2'-enyl)furan-2-ol

: 213262-40-9
(2R,3S)-5-Benzenesulfonyl-3-methyl-2-((S)-1-methyl-allyl)-tetrahydro-furan

Guidance literature:: With calcium chloride; In dichloromethane;
DOI:10.1016/S0040-4039(00)76542-7

Reference yield:

: 106357-24-8
(3S,4S,5S)-6-(tert-butyldiphenylsiloxy)-4-hydroxy-3,5-dimethylhexan-1-ene

: 213262-40-9
(2R,3S)-5-Benzenesulfonyl-3-methyl-2-((S)-1-methyl-allyl)-tetrahydro-furan

Guidance literature:: Multi-step reaction with 5 steps

1: 100 percent / nBu₄NF / tetrahydrofuran

2: 94 percent / Et₃N / CH₂Cl₂

3: 97 percent / dimethylsulfoxide / 60 °C

4: 94 percent / DIBAL-H / toluene / -78 °C

5: 93 percent / CaCl₂ / CH₂Cl₂

With tetrabutyl ammonium fluoride; diisobutylaluminium hydride; triethylamine; calcium chloride; In tetrahydrofuran; dichloromethane; dimethyl sulfoxide; toluene;
DOI:10.1016/S0040-4039(00)76542-7

Reference yield:

: 155417-64-4
(2S,3S,4S)-2,4-Dimethylhex-5-ene-1,3-diol

: 213262-40-9
(2R,3S)-5-Benzenesulfonyl-3-methyl-2-((S)-1-methyl-allyl)-tetrahydro-furan

Guidance literature:: Multi-step reaction with 4 steps

1: 94 percent / Et₃N / CH₂Cl₂

2: 97 percent / dimethylsulfoxide / 60 °C

3: 94 percent / DIBAL-H / toluene / -78 °C

4: 93 percent / CaCl₂ / CH₂Cl₂

With diisobutylaluminium hydride; triethylamine; calcium chloride; In dichloromethane; dimethyl sulfoxide; toluene;
DOI:10.1016/S0040-4039(00)76542-7