(+)-5R-(1-Hydroxy-1-methyl ethyl)-3S-(N-acetylaminomethyl)-2-methylcyclohexanone

Base Information

Chemical Name:(+)-5R-(1-Hydroxy-1-methyl ethyl)-3S-(N-acetylaminomethyl)-2-methylcyclohexanone
CAS No.:143023-78-3
Molecular Formula:C₁₃H₂₃NO₃
Molecular Weight:241.331
Hs Code.:

Synonyms:(+)-5R-(1-Hydroxy-1-methyl ethyl)-3S-(N-acetylaminomethyl)-2-methylcyclohexanone

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Chemical Property of (+)-5R-(1-Hydroxy-1-methyl ethyl)-3S-(N-acetylaminomethyl)-2-methylcyclohexanone

Chemical Property:

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Technology Process of (+)-5R-(1-Hydroxy-1-methyl ethyl)-3S-(N-acetylaminomethyl)-2-methylcyclohexanone

There total 5 articles about (+)-5R-(1-Hydroxy-1-methyl ethyl)-3S-(N-acetylaminomethyl)-2-methylcyclohexanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 143023-77-2
9R-(1-Hydroxy-1-methyl ethyl)-7S-(N-acetylaminomethyl)-1,4-dioxaspiro<4.5> decane

: 143023-78-3
(+)-5R-(1-Hydroxy-1-methyl ethyl)-3S-(N-acetylaminomethyl)-2-methylcyclohexanone

Guidance literature:: With hydrogenchloride; In acetone; Ambient temperature;

Reference yield:

: 137625-67-3
(-)-(1R,2R,5R)-2-methyl-5-(1-methylethenyl)-3-oxocyclohexanecarbonitrile

: 143023-78-3
(+)-5R-(1-Hydroxy-1-methyl ethyl)-3S-(N-acetylaminomethyl)-2-methylcyclohexanone

Guidance literature:: Multi-step reaction with 5 steps

1: 87 percent / H₂SO₄/H₂O

2: 59 percent / p-TsOH / benzene / 2.5 h / Heating

3: 100 percent / KOH / 2-methyl-propan-2-ol / 14.5 h / Heating

4: 83 percent / Et₃N / CH₂Cl₂ / 0 °C

5: 80 percent / 6N HCl / acetone / Ambient temperature

With hydrogenchloride; potassium hydroxide; sulfuric acid; water; toluene-4-sulfonic acid; triethylamine; In dichloromethane; acetone; tert-butyl alcohol; benzene;

Reference yield:

: 137588-59-1
(-)-(1R,2R,5R)-2-methyl-5-(1-hydroxy-1-methylethyl)-3-oxocyclohexanecarbonitrile

: 143023-78-3
(+)-5R-(1-Hydroxy-1-methyl ethyl)-3S-(N-acetylaminomethyl)-2-methylcyclohexanone

Guidance literature:: Multi-step reaction with 4 steps

1: 59 percent / p-TsOH / benzene / 2.5 h / Heating

2: 100 percent / KOH / 2-methyl-propan-2-ol / 14.5 h / Heating

3: 83 percent / Et₃N / CH₂Cl₂ / 0 °C

4: 80 percent / 6N HCl / acetone / Ambient temperature

With hydrogenchloride; potassium hydroxide; toluene-4-sulfonic acid; triethylamine; In dichloromethane; acetone; tert-butyl alcohol; benzene;