Technology Process of C28H28(2)HN3O2S
There total 4 articles about C28H28(2)HN3O2S which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
C28H28(2)HN3O2S;
With
lithium hexamethyldisilazane;
In
tetrahydrofuran; ethylbenzene;
at -78 - 20 ℃;
for 4h;
Inert atmosphere;
With
water;
In
tetrahydrofuran; ethylbenzene;
at 20 ℃;
regioselective reaction;
Inert atmosphere;
DOI:10.1021/ja211486f
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: lithium aluminium deuteride / dichloromethane / Inert atmosphere
2.1: dichloromethane / Inert atmosphere
3.1: triphenylphosphine; diethylazodicarboxylate / tetrahydrofuran / Inert atmosphere
4.1: copper(l) iodide / acetonitrile / 16 h / 20 °C / Inert atmosphere
5.1: lithium hexamethyldisilazane / tetrahydrofuran; ethylbenzene / 4 h / -78 - 20 °C / Inert atmosphere
5.2: 20 °C / Inert atmosphere
With
copper(l) iodide; lithium aluminium deuteride; triphenylphosphine; lithium hexamethyldisilazane; diethylazodicarboxylate;
In
tetrahydrofuran; dichloromethane; ethylbenzene; acetonitrile;
DOI:10.1021/ja211486f
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: triphenylphosphine; diethylazodicarboxylate / tetrahydrofuran / Inert atmosphere
2.1: copper(l) iodide / acetonitrile / 16 h / 20 °C / Inert atmosphere
3.1: lithium hexamethyldisilazane / tetrahydrofuran; ethylbenzene / 4 h / -78 - 20 °C / Inert atmosphere
3.2: 20 °C / Inert atmosphere
With
copper(l) iodide; triphenylphosphine; lithium hexamethyldisilazane; diethylazodicarboxylate;
In
tetrahydrofuran; ethylbenzene; acetonitrile;
DOI:10.1021/ja211486f
