C₅₃H₇₃NO₁₁*ClH

Base Information

Chemical Name:C₅₃H₇₃NO₁₁*ClH
CAS No.:1188547-54-7
Molecular Formula:C₅₃H₇₃NO₁₁*ClH
Molecular Weight:936.624
Hs Code.:

C<sub>53</sub>H<sub>73</sub>NO<sub>11</sub>*ClH

Synonyms:C₅₃H₇₃NO₁₁*ClH

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Chemical Property of C₅₃H₇₃NO₁₁*ClH

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Technology Process of C₅₃H₇₃NO₁₁*ClH

There total 18 articles about C₅₃H₇₃NO₁₁*ClH which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1188547-53-6
C₅₈H₈₁NO₁₂

: 1188547-54-7
C₅₃H₇₃NO₁₁*ClH

Guidance literature:: With hydrogenchloride; In tetrahydrofuran; methanol; water; at 20 ℃; for 12h;
DOI:10.1021/ja905924u

Reference yield:

: 58574-03-1
4'-Hydroxybiphenyl-4-carboxylic acid

: 1188547-54-7
C₅₃H₇₃NO₁₁*ClH

Guidance literature:: Multi-step reaction with 6 steps

1: sulfuric acid / 0 °C / Reflux

2: potassium carbonate / N,N-dimethyl-formamide / 72 h / 90 °C

3: 1-methyl-piperazine; sodium bis(2-methoxyethoxy)aluminium dihydride / toluene / 8 h / 0 °C / Inert atmosphere

4: benzene / 24 h / 100 °C

5: methanol; sodium tetrahydroborate / 12 h / 20 °C

6: hydrogenchloride; water / tetrahydrofuran; methanol / 12 h / 20 °C

With 1-methyl-piperazine; hydrogenchloride; methanol; sodium tetrahydroborate; sulfuric acid; water; potassium carbonate; sodium bis(2-methoxyethoxy)aluminium dihydride; In tetrahydrofuran; methanol; N,N-dimethyl-formamide; toluene; benzene;

Reference yield:

: 134-96-3
syringic aldehyde

: 1188547-54-7
C₅₃H₇₃NO₁₁*ClH

Guidance literature:: Multi-step reaction with 7 steps

1.1: hydroxylamine hydrochloride; sodium acetate / methanol / 2 h / Reflux

2.1: acetic anhydride / Reflux

2.2: 24 h / 20 °C

3.1: potassium carbonate / N,N-dimethyl-formamide / 72 h / 90 °C

4.1: lithium aluminium tetrahydride / tetrahydrofuran / 12 h / 0 - 87 °C / Inert atmosphere

4.2: 0 °C

5.1: benzene / 24 h / 100 °C

6.1: methanol; sodium tetrahydroborate / 12 h / 20 °C

7.1: hydrogenchloride; water / tetrahydrofuran; methanol / 12 h / 20 °C

With hydrogenchloride; methanol; sodium tetrahydroborate; lithium aluminium tetrahydride; hydroxylamine hydrochloride; water; sodium acetate; acetic anhydride; potassium carbonate; In tetrahydrofuran; methanol; N,N-dimethyl-formamide; benzene;