Technology Process of C23H26O5S
There total 1 articles about C23H26O5S which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
(p-methylphenyl) 4,6-O-benzylidene-1-thio-β-D-galactopyranoside;
With
di(n-butyl)tin oxide;
In
toluene;
for 4h;
Inert atmosphere;
Reflux;
allyl bromide;
With
tetra-(n-butyl)ammonium iodide; cesium fluoride;
In
N,N-dimethyl-formamide;
Inert atmosphere;
Reflux;
DOI:10.1039/c0ob00990c
- Guidance literature:
-
C23H26O5S;
With
tetra-(n-butyl)ammonium iodide; sodium hydride;
In
N,N-dimethyl-formamide;
at 0 ℃;
for 0.166667h;
Inert atmosphere;
p-methoxybenzyl chloride;
In
N,N-dimethyl-formamide;
at 0 - 20 ℃;
for 4h;
Inert atmosphere;
DOI:10.1039/c0ob00990c
- Guidance literature:
-
Multi-step reaction with 7 steps
1.1: tetra-(n-butyl)ammonium iodide; sodium hydride / N,N-dimethyl-formamide / 0.17 h / 0 °C / Inert atmosphere
1.2: 4 h / 0 - 20 °C / Inert atmosphere
2.1: trimethylsilyl iodide / dichloromethane / 0.17 h / 0 °C / Molecular sieve; Inert atmosphere
3.1: tetra-(n-butyl)ammonium iodide; N-ethyl-N,N-diisopropylamine / toluene / 3 h / 80 °C / Inert atmosphere; Molecular sieve
4.1: piperidine / dichloromethane / 0.33 h / 20 °C / Inert atmosphere
5.1: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine / dichloromethane / 3 h / 20 °C / Inert atmosphere
6.1: 4-methyl-morpholine; tetrakis(triphenylphosphine) palladium(0) / tetrahydrofuran / 2 h / 20 °C / Inert atmosphere
6.2: Inert atmosphere
7.1: 4-methyl-morpholine; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 2 h / 20 °C / Inert atmosphere
With
piperidine; 4-methyl-morpholine; tetrakis(triphenylphosphine) palladium(0); trimethylsilyl iodide; tetra-(n-butyl)ammonium iodide; sodium hydride; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; N-ethyl-N,N-diisopropylamine;
In
tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide; toluene;
DOI:10.1039/c0ob00990c
