3-(4-methoxyphenyl)-1-[2,4,6-tris(benzyloxy)phenyl]-[1,2,3-⁽¹³⁾C₃]-2-propen-1-one

Base Information

• Chemical Name: 3-(4-methoxyphenyl)-1-[2,4,6-tris(benzyloxy)phenyl]-[1,2,3-⁽¹³⁾C₃]-2-propen-1-one
• CAS No.: 1229516-40-8
• Molecular Formula: C₃₇H₃₂O₅
• Molecular Weight: 559.625

Synonyms:3-(4-methoxyphenyl)-1-[2,4,6-tris(benzyloxy)phenyl]-[1,2,3-⁽¹³⁾C₃]-2-propen-1-one

Chemical Property of 3-(4-methoxyphenyl)-1-[2,4,6-tris(benzyloxy)phenyl]-[1,2,3-⁽¹³⁾C₃]-2-propen-1-one

Chemical Property:

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Technology Process of 3-(4-methoxyphenyl)-1-[2,4,6-tris(benzyloxy)phenyl]-[1,2,3-⁽¹³⁾C₃]-2-propen-1-one

There total 6 articles about 3-(4-methoxyphenyl)-1-[2,4,6-tris(benzyloxy)phenyl]-[1,2,3-⁽¹³⁾C₃]-2-propen-1-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

2,4,6-[1',2'-(13)C2]tribenzyloxyacetophenone (1229516-38-4) + α-[13C]-4-methoxybenzaldehyde (95537-93-2) → 3-(4-methoxyphenyl)-1-[2,4,6-tris(benzyloxy)phenyl]-[1,2,3-(13)C3]-2-propen-1-one (1229516-40-8)

Guidance literature:

With potassium hydroxide; In ethanol; for 8h; Inert atmosphere; Reflux;

DOI:10.1002/jlcr.1732

Reference yield:

3,5-dimethoxyphenol (500-99-2) → 3-(4-methoxyphenyl)-1-[2,4,6-tris(benzyloxy)phenyl]-[1,2,3-(13)C3]-2-propen-1-one (1229516-40-8)

Guidance literature:

Multi-step reaction with 4 steps

1.1: boron trichloride / dichloromethane / 0.08 h / -10 °C

1.2: Reflux

2.1: boron tribromide / dichloromethane / 24 h / 20 °C / Inert atmosphere

2.2: 3 h / Reflux

3.1: 18-crown-6 ether; potassium carbonate / acetone / 8 h / 60 °C

4.1: potassium hydroxide / ethanol / 8 h / Inert atmosphere; Reflux

With 18-crown-6 ether; boron trichloride; boron tribromide; potassium carbonate; potassium hydroxide; In ethanol; dichloromethane; acetone;

DOI:10.1002/jlcr.1732

Reference yield:

(13C)-4-methoxybenzonitrile (1333245-00-3) → 3-(4-methoxyphenyl)-1-[2,4,6-tris(benzyloxy)phenyl]-[1,2,3-(13)C3]-2-propen-1-one (1229516-40-8)

Guidance literature:

Multi-step reaction with 2 steps

1: diisobutylaluminium hydride / tetrahydrofuran / 20 °C

2: potassium hydroxide / ethanol / 8 h / Inert atmosphere; Reflux

With diisobutylaluminium hydride; potassium hydroxide; In tetrahydrofuran; ethanol;

DOI:10.1002/jlcr.1732

upstream raw materials:

benzyl bromide

3,5-dimethoxyphenol

2,4,6-[1',2'-⁽¹³⁾C₂]tribenzyloxyacetophenone

α-[¹³C]-4-methoxybenzaldehyde

Downstream raw materials:

[2,3,4-⁽¹³⁾C₃]biochanin A

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