N-[4-(2,3,4,6-tetra-O-acetyl-α-D-mannopyranosyloxy)phenyl]acetyl-L-cysteine [2-(2,3,4,6-tetra-O-acetyl-α-D-mannopyranosyloxy)ethyl]amide

Base Information

• Chemical Name: N-[4-(2,3,4,6-tetra-O-acetyl-α-D-mannopyranosyloxy)phenyl]acetyl-L-cysteine [2-(2,3,4,6-tetra-O-acetyl-α-D-mannopyranosyloxy)ethyl]amide
• CAS No.: 1234673-35-8
• Molecular Formula: C₄₁H₅₄N₂O₂₂S
• Molecular Weight: 958.946

Synonyms:N-[4-(2,3,4,6-tetra-O-acetyl-α-D-mannopyranosyloxy)phenyl]acetyl-L-cysteine [2-(2,3,4,6-tetra-O-acetyl-α-D-mannopyranosyloxy)ethyl]amide

Chemical Property of N-[4-(2,3,4,6-tetra-O-acetyl-α-D-mannopyranosyloxy)phenyl]acetyl-L-cysteine [2-(2,3,4,6-tetra-O-acetyl-α-D-mannopyranosyloxy)ethyl]amide

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Technology Process of N-[4-(2,3,4,6-tetra-O-acetyl-α-D-mannopyranosyloxy)phenyl]acetyl-L-cysteine [2-(2,3,4,6-tetra-O-acetyl-α-D-mannopyranosyloxy)ethyl]amide

There total 1 articles about N-[4-(2,3,4,6-tetra-O-acetyl-α-D-mannopyranosyloxy)phenyl]acetyl-L-cysteine [2-(2,3,4,6-tetra-O-acetyl-α-D-mannopyranosyloxy)ethyl]amide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

N-[4-(2,3,4,6-tetra-O-acetyl-α-D-mannopyranosyloxy)phenyl]acetyl-S-(triphenylmethyl)-L-cysteine [2-(2,3,4,6-tetra-O-acetyl-α-D-mannopyranosyloxy)ethyl]amide (1234673-34-7) → N-[4-(2,3,4,6-tetra-O-acetyl-α-D-mannopyranosyloxy)phenyl]acetyl-L-cysteine [2-(2,3,4,6-tetra-O-acetyl-α-D-mannopyranosyloxy)ethyl]amide (1234673-35-8)

Guidance literature:

With triethylsilane; trifluoroacetic acid; In dichloromethane; at 20 ℃; for 2h; Inert atmosphere;

DOI:10.1002/ejoc.201000185

Reference yield: 34.0%

4-(bromomethyl)phenyl 2,3,4,6-tetra-O-acetyl-α-D-mannopyranoside (1234673-36-9) + N-[4-(2,3,4,6-tetra-O-acetyl-α-D-mannopyranosyloxy)phenyl]acetyl-L-cysteine [2-(2,3,4,6-tetra-O-acetyl-α-D-mannopyranosyloxy)ethyl]amide (1234673-35-8) → N-[4-(2,3,4,6-tetra-O-acetyl-α-D-mannopyranosyloxy)phenyl]acetyl-S-[4-(2,3,4,6-tetra-O-acetyl-α-D-mannopyranosyl)benzyl]-L-cysteine [2-(2,3,4,6-tetra-O-acetyl-α-D-mannopyranosyloxy)ethyl]amide

Guidance literature:

With sodium hydride; In N,N-dimethyl-formamide; at 20 ℃; for 3h; Ultrasound;

DOI:10.1002/ejoc.201000185

upstream raw materials:

N-[4-(2,3,4,6-tetra-O-acetyl-α-D-mannopyranosyloxy)phenyl]acetyl-S-(triphenylmethyl)-L-cysteine [2-(2,3,4,6-tetra-O-acetyl-α-D-mannopyranosyloxy)ethyl]amide

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