ethyl 2-[(E)-2-bromo-3-methoxy-3-oxo-1-phenylprop-1-enylimino]-3-oxobutanoate

Base Information

Chemical Name:ethyl 2-[(E)-2-bromo-3-methoxy-3-oxo-1-phenylprop-1-enylimino]-3-oxobutanoate
CAS No.:1403871-49-7
Molecular Formula:C₁₆H₁₆BrNO₅
Molecular Weight:382.211
Hs Code.:

Synonyms:ethyl 2-[(E)-2-bromo-3-methoxy-3-oxo-1-phenylprop-1-enylimino]-3-oxobutanoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of ethyl 2-[(E)-2-bromo-3-methoxy-3-oxo-1-phenylprop-1-enylimino]-3-oxobutanoate

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Technology Process of ethyl 2-[(E)-2-bromo-3-methoxy-3-oxo-1-phenylprop-1-enylimino]-3-oxobutanoate

There total 3 articles about ethyl 2-[(E)-2-bromo-3-methoxy-3-oxo-1-phenylprop-1-enylimino]-3-oxobutanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

: 2009-97-4
ethyl 2-diazo-3-oxobutanoate

: 367967-56-4
methyl 2-bromo-3-phenyl-2H-azirine-2-carboxylate

: 1403871-49-7
ethyl 2-[(E)-2-bromo-3-methoxy-3-oxo-1-phenylprop-1-enylimino]-3-oxobutanoate

Guidance literature:: With dirhodium tetraacetate; In 1,2-dichloro-ethane; at 84 ℃; for 0.00833333h; stereoselective reaction; Inert atmosphere;
DOI:10.1039/c6ob00588h

Reference yield: 43.0%

: 2009-97-4
ethyl 2-diazo-3-oxobutanoate

: 367967-56-4
methyl 2-bromo-3-phenyl-2H-azirine-2-carboxylate

: C₁₆H₁₆BrNO₅

: C₁₆H₁₆BrNO₅

: 1403871-49-7
ethyl 2-[(E)-2-bromo-3-methoxy-3-oxo-1-phenylprop-1-enylimino]-3-oxobutanoate

Guidance literature:: With dirhodium tetraacetate; In 1,2-dichloro-ethane; at 84 ℃; stereoselective reaction; Inert atmosphere;
DOI:10.1016/j.tetlet.2012.08.063

Reference yield: 43.0%

: 2009-97-4
ethyl 2-diazo-3-oxobutanoate

: 367967-56-4
methyl 2-bromo-3-phenyl-2H-azirine-2-carboxylate

: 1403871-49-7
ethyl 2-[(E)-2-bromo-3-methoxy-3-oxo-1-phenylprop-1-enylimino]-3-oxobutanoate

: 2-ethyl 3-methyl 2-acetyl-3-bromo-4-phenyl-2,3-dihydroazete-2,3-dicarboxylate

Guidance literature:: With dirhodium tetraacetate; In 1,2-dichloro-ethane; stereoselective reaction; Inert atmosphere; Reflux;
DOI:10.1016/j.tet.2015.05.022