(R)-(R)-1-(4-(diethyl(3-methyl-4-(((R)-3,3,3-trifluoro-2-methoxy-2-phenylpropanoyl)oxy)phenyl)silyl)-2-methylphenoxy)-3,3-dimethylbutan-2-yl-3,3,3-trifluoro-2-methoxy-2-phenylpropanoate

Base Information

Chemical Name:(R)-(R)-1-(4-(diethyl(3-methyl-4-(((R)-3,3,3-trifluoro-2-methoxy-2-phenylpropanoyl)oxy)phenyl)silyl)-2-methylphenoxy)-3,3-dimethylbutan-2-yl-3,3,3-trifluoro-2-methoxy-2-phenylpropanoate
CAS No.:1427540-91-7
Molecular Formula:C₄₄H₅₀F₆O₇Si
Molecular Weight:832.953
Hs Code.:

(R)-(R)-1-(4-(diethyl(3-methyl-4-(((R)-3,3,3-trifluoro-2-methoxy-2-phenylpropanoyl)oxy)phenyl)silyl)-2-methylphenoxy)-3,3-dimethylbutan-2-yl-3,3,3-trifluoro-2-methoxy-2-phenylpropanoate

Synonyms:(R)-(R)-1-(4-(diethyl(3-methyl-4-(((R)-3,3,3-trifluoro-2-methoxy-2-phenylpropanoyl)oxy)phenyl)silyl)-2-methylphenoxy)-3,3-dimethylbutan-2-yl-3,3,3-trifluoro-2-methoxy-2-phenylpropanoate

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Chemical Property of (R)-(R)-1-(4-(diethyl(3-methyl-4-(((R)-3,3,3-trifluoro-2-methoxy-2-phenylpropanoyl)oxy)phenyl)silyl)-2-methylphenoxy)-3,3-dimethylbutan-2-yl-3,3,3-trifluoro-2-methoxy-2-phenylpropanoate

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Technology Process of (R)-(R)-1-(4-(diethyl(3-methyl-4-(((R)-3,3,3-trifluoro-2-methoxy-2-phenylpropanoyl)oxy)phenyl)silyl)-2-methylphenoxy)-3,3-dimethylbutan-2-yl-3,3,3-trifluoro-2-methoxy-2-phenylpropanoate

There total 2 articles about (R)-(R)-1-(4-(diethyl(3-methyl-4-(((R)-3,3,3-trifluoro-2-methoxy-2-phenylpropanoyl)oxy)phenyl)silyl)-2-methylphenoxy)-3,3-dimethylbutan-2-yl-3,3,3-trifluoro-2-methoxy-2-phenylpropanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1427540-75-7
C₂₄H₃₆O₃Si

: 39637-99-5,20445-33-4
(S)-(+)-2-methoxy-2-trifluoromethyl-2-phenylacetyl chloride

: 1427540-91-7
(R)-(R)-1-(4-(diethyl(3-methyl-4-(((R)-3,3,3-trifluoro-2-methoxy-2-phenylpropanoyl)oxy)phenyl)silyl)-2-methylphenoxy)-3,3-dimethylbutan-2-yl-3,3,3-trifluoro-2-methoxy-2-phenylpropanoate

Guidance literature:: With pyridine; In dichloromethane; at 20 ℃; for 20h;
DOI:10.1016/j.bmc.2013.01.060

Reference yield:

: 1247016-21-2
1-(4-(diethyl(4-hydroxy-3-methylphenyl)silyl)-2-methylphenoxy)-3,3-dimethylbutan-2-one

: 1427540-91-7
(R)-(R)-1-(4-(diethyl(3-methyl-4-(((R)-3,3,3-trifluoro-2-methoxy-2-phenylpropanoyl)oxy)phenyl)silyl)-2-methylphenoxy)-3,3-dimethylbutan-2-yl-3,3,3-trifluoro-2-methoxy-2-phenylpropanoate

Guidance literature:: Multi-step reaction with 2 steps

1: borane N-ethyl-N-isopropylaniline complex; (3aR)-1-methyl-3,3-diphenyl-tetrahydro-pyrrolo[1,2-c][1,3,2]oxazaborole / tetrahydrofuran; toluene / 1 h / 20 °C / Inert atmosphere

2: pyridine / dichloromethane / 20 h / 20 °C

With pyridine; borane N-ethyl-N-isopropylaniline complex; (3aR)-1-methyl-3,3-diphenyl-tetrahydro-pyrrolo[1,2-c][1,3,2]oxazaborole; In tetrahydrofuran; dichloromethane; toluene; 1: |Corey-Bakshi-Shibata Reduction;
DOI:10.1016/j.bmc.2013.01.060