(1R,1'R)-1,1'-((2R,2'R,5R,5'R)-octahydro-2,2'-bifuran-5,5'-diyl)-bis(6-(4-(n-butyl)phenoxy)hex-3-yn-1-ol)

Base Information

• Chemical Name: (1R,1'R)-1,1'-((2R,2'R,5R,5'R)-octahydro-2,2'-bifuran-5,5'-diyl)-bis(6-(4-(n-butyl)phenoxy)hex-3-yn-1-ol)
• CAS No.: 839674-19-0
• Molecular Formula: C₄₀H₅₄O₆
• Molecular Weight: 630.865

Synonyms:(1R,1'R)-1,1'-((2R,2'R,5R,5'R)-octahydro-2,2'-bifuran-5,5'-diyl)-bis(6-(4-(n-butyl)phenoxy)hex-3-yn-1-ol)

Chemical Property of (1R,1'R)-1,1'-((2R,2'R,5R,5'R)-octahydro-2,2'-bifuran-5,5'-diyl)-bis(6-(4-(n-butyl)phenoxy)hex-3-yn-1-ol)

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Technology Process of (1R,1'R)-1,1'-((2R,2'R,5R,5'R)-octahydro-2,2'-bifuran-5,5'-diyl)-bis(6-(4-(n-butyl)phenoxy)hex-3-yn-1-ol)

There total 1 articles about (1R,1'R)-1,1'-((2R,2'R,5R,5'R)-octahydro-2,2'-bifuran-5,5'-diyl)-bis(6-(4-(n-butyl)phenoxy)hex-3-yn-1-ol) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

1-(but-3-ynyloxy)-4-(n-butyl)benzene (839674-18-9) + (-)-(2R,3R,6R,7R,10R,11R)-1,2:3,6:7,10:11,12-tetraepoxydodecane (173427-88-8) → (1R,1'R)-1,1'-((2R,2'R,5R,5'R)-octahydro-2,2'-bifuran-5,5'-diyl)-bis(6-(4-(n-butyl)phenoxy)hex-3-yn-1-ol) (839674-19-0)

Guidance literature:

1-(but-3-ynyloxy)-4-(n-butyl)benzene; With n-butyllithium; In tetrahydrofuran; hexane; at -78 ℃; for 0.5h;

With boron trifluoride diethyl etherate; In tetrahydrofuran; hexane; for 0.5h;

(-)-(2R,3R,6R,7R,10R,11R)-1,2:3,6:7,10:11,12-tetraepoxydodecane; Further stages;

DOI:10.1016/j.bmc.2008.10.071

Reference yield: 87.0%

(1R,1'R)-1,1'-((2R,2'R,5R,5'R)-octahydro-2,2'-bifuran-5,5'-diyl)-bis(6-(4-(n-butyl)phenoxy)hex-3-yn-1-ol) (839674-19-0) → (1R,1'R)-1,1'-((2R,2'R,5R,5'R)-octahydro-2,2'-bifuran-5,5'-diyl)-bis(6-(4-(n-butyl)phenoxy)hexan-1-ol)

Guidance literature:

With palladium 10% on activated carbon; hydrogen; In ethanol; at 20 ℃;

DOI:10.1016/j.bmc.2008.10.071

upstream raw materials:

1-(but-3-ynyloxy)-4-(n-butyl)benzene

(-)-(2R,3R,6R,7R,10R,11R)-1,2:3,6:7,10:11,12-tetraepoxydodecane

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