1-(tert-butoxyformamido)-2,2-dibromo-1-(3-bromo-4-methoxyphenyl)-2-nitroethane

Base Information

Chemical Name:1-(tert-butoxyformamido)-2,2-dibromo-1-(3-bromo-4-methoxyphenyl)-2-nitroethane
CAS No.:1420743-18-5
Molecular Formula:C₁₄H₁₇Br₃N₂O₅
Molecular Weight:533.011
Hs Code.:

Synonyms:1-(tert-butoxyformamido)-2,2-dibromo-1-(3-bromo-4-methoxyphenyl)-2-nitroethane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-(tert-butoxyformamido)-2,2-dibromo-1-(3-bromo-4-methoxyphenyl)-2-nitroethane

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Technology Process of 1-(tert-butoxyformamido)-2,2-dibromo-1-(3-bromo-4-methoxyphenyl)-2-nitroethane

There total 2 articles about 1-(tert-butoxyformamido)-2,2-dibromo-1-(3-bromo-4-methoxyphenyl)-2-nitroethane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 70400-19-0
C₉H₈BrNO₃

: 358365-86-3
tert-butyl N,N-dibromocarbamate

: 1420743-18-5
1-(tert-butoxyformamido)-2,2-dibromo-1-(3-bromo-4-methoxyphenyl)-2-nitroethane

Guidance literature:: With potassium phosphate tribasic trihydrate; In dichloromethane; at 20 ℃; for 1h;
DOI:10.1021/jo302727v

Reference yield:

: 4248-19-5
tert-butyl carbazate

: 1420743-18-5
1-(tert-butoxyformamido)-2,2-dibromo-1-(3-bromo-4-methoxyphenyl)-2-nitroethane

Guidance literature:: Multi-step reaction with 2 steps

1: sodium hydroxide; bromine / water / 2 h / 20 °C

2: potassium phosphate tribasic trihydrate / dichloromethane / 1 h / 20 °C

With potassium phosphate tribasic trihydrate; bromine; sodium hydroxide; In dichloromethane; water;
DOI:10.1021/jo302727v