5-[(6-chloro-4-pyrimidinyl)amino]-2-methoxy-phenol hydrochloric acid salt

Base Information

• Chemical Name: 5-[(6-chloro-4-pyrimidinyl)amino]-2-methoxy-phenol hydrochloric acid salt
• CAS No.: 892414-15-2
• Molecular Formula: C₁₁H₁₀ClN₃O₂*ClH
• Molecular Weight: 288.133

Synonyms:5-[(6-chloro-4-pyrimidinyl)amino]-2-methoxy-phenol hydrochloric acid salt

Chemical Property of 5-[(6-chloro-4-pyrimidinyl)amino]-2-methoxy-phenol hydrochloric acid salt

Chemical Property:

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Technology Process of 5-[(6-chloro-4-pyrimidinyl)amino]-2-methoxy-phenol hydrochloric acid salt

There total 1 articles about 5-[(6-chloro-4-pyrimidinyl)amino]-2-methoxy-phenol hydrochloric acid salt which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

5-(6-chloro-pyrimidin-4-ylamino)-2-methoxy-phenol (892545-89-0) → 5-[(6-chloro-4-pyrimidinyl)amino]-2-methoxy-phenol hydrochloric acid salt (892414-15-2)

Guidance literature:

With hydrogenchloride; In isopropyl alcohol;

Reference yield: 55.0%

5-[(6-chloro-4-pyrimidinyl)amino]-2-methoxy-phenol hydrochloric acid salt (892414-15-2) + 3-aminobenzenemethanol (1877-77-6) → 3-[[6-[(3-hydroxy-4-methoxyphenyl)amino]-4-pyrimidinyl]amino]-benzenemethanol (892413-86-4)

Guidance literature:

With hydrogenchloride; In isopropyl alcohol; butan-1-ol; at 130 ℃; Microwave;

Reference yield:

5-[(6-chloro-4-pyrimidinyl)amino]-2-methoxy-phenol hydrochloric acid salt (892414-15-2) + 4-chloro-5-hydroxymethyl aniline (89951-56-4) → C18H17ClN4O3 (892414-17-4)

Guidance literature:

In N,N-dimethyl-formamide; at 140 ℃; for 5h;

upstream raw materials:

5-(6-chloro-pyrimidin-4-ylamino)-2-methoxy-phenol

Downstream raw materials:

3-[[6-[(3-hydroxy-4-methoxyphenyl)amino]-4-pyrimidinyl]amino]-benzenemethanol

C₁₈H₁₇ClN₄O₃

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