N-<1(S)-ethoxycarbonyl-6-(1-benzyloxycarbonyl-4-piperidyl)hexyl>-L-alanine tert-butyl ester

Base Information

Chemical Name:N-<1(S)-ethoxycarbonyl-6-(1-benzyloxycarbonyl-4-piperidyl)hexyl>-L-alanine tert-butyl ester
CAS No.:120008-77-7
Molecular Formula:C₂₉H₄₆N₂O₆
Molecular Weight:518.694
Hs Code.:

Synonyms:N-<1(S)-ethoxycarbonyl-6-(1-benzyloxycarbonyl-4-piperidyl)hexyl>-L-alanine tert-butyl ester

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Chemical Property of N-<1(S)-ethoxycarbonyl-6-(1-benzyloxycarbonyl-4-piperidyl)hexyl>-L-alanine tert-butyl ester

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Technology Process of N-<1(S)-ethoxycarbonyl-6-(1-benzyloxycarbonyl-4-piperidyl)hexyl>-L-alanine tert-butyl ester

There total 1 articles about N-<1(S)-ethoxycarbonyl-6-(1-benzyloxycarbonyl-4-piperidyl)hexyl>-L-alanine tert-butyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 13404-22-3
tert-butyl L-alaninate hydrochloride

: 99198-68-2
ethyl 7-(1-benzyloxycarbonyl-4-piperidyl)-2-oxoheptanoate

: 129389-21-5
N-<1(R)-ethoxycarbonyl-6-(1-benzyloxycarbonyl-4-piperidyl)hexyl>-L-alanine tert-butyl ester

: 120008-77-7
N-<1(S)-ethoxycarbonyl-6-(1-benzyloxycarbonyl-4-piperidyl)hexyl>-L-alanine tert-butyl ester

Guidance literature:: With molecular sieve; sodium cyanoborohydride; Yield given. Multistep reaction; 1) EtOH, 1 h;

Reference yield: 84.0%

: 120008-77-7
N-<1(S)-ethoxycarbonyl-6-(1-benzyloxycarbonyl-4-piperidyl)hexyl>-L-alanine tert-butyl ester

: 120008-92-6
N-<1(S)-ethoxycarbonyl-6-(1-benzyloxycarbonyl-4-piperidyl)hexyl>-L-alanine

Guidance literature:: With formic acid; at 40 ℃; for 30h;

Reference yield:

: 120008-77-7
N-<1(S)-ethoxycarbonyl-6-(1-benzyloxycarbonyl-4-piperidyl)hexyl>-L-alanine tert-butyl ester

: 120008-78-8
N-<1(S)-ethoxycarbonyl-6-(1-benzyloxycarbonyl-4-piperidyl)hexyl>-L-alanyl-L-proline benzyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 84 percent / 99percent formic acid / 30 h / 40 °C

2: 96 percent / diethyl phosphorocyanidate, Et₃N / dimethylformamide / 3 h

With formic acid; diethyl cyanophosphonate; triethylamine; In N,N-dimethyl-formamide;