4-chlorobenzyl 4-[2-(1H-benzotriazol-5-ylcarbamoyl)ethyl-carbamoyl]piperidine-1-carboxylate

Base Information

Chemical Name:4-chlorobenzyl 4-[2-(1H-benzotriazol-5-ylcarbamoyl)ethyl-carbamoyl]piperidine-1-carboxylate
CAS No.:1246639-72-4
Molecular Formula:C₂₃H₂₅ClN₆O₄
Molecular Weight:484.942
Hs Code.:

Synonyms:4-chlorobenzyl 4-[2-(1H-benzotriazol-5-ylcarbamoyl)ethyl-carbamoyl]piperidine-1-carboxylate

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Chemical Property of 4-chlorobenzyl 4-[2-(1H-benzotriazol-5-ylcarbamoyl)ethyl-carbamoyl]piperidine-1-carboxylate

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Technology Process of 4-chlorobenzyl 4-[2-(1H-benzotriazol-5-ylcarbamoyl)ethyl-carbamoyl]piperidine-1-carboxylate

There total 5 articles about 4-chlorobenzyl 4-[2-(1H-benzotriazol-5-ylcarbamoyl)ethyl-carbamoyl]piperidine-1-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 32.0%

: 1246640-04-9
C₁₅H₂₀N₆O₂

: 873-76-7
para-Chlorobenzyl alcohol

: 530-62-1
1,1'-carbonyldiimidazole

: 1246639-72-4
4-chlorobenzyl 4-[2-(1H-benzotriazol-5-ylcarbamoyl)ethyl-carbamoyl]piperidine-1-carboxylate

Guidance literature:: para-Chlorobenzyl alcohol; 1,1'-carbonyldiimidazole; In N,N-dimethyl-formamide; at 20 ℃; for 2h;

C₁₅H₂₀N₆O₂; In N,N-dimethyl-formamide; at 20 ℃; for 16h;

Reference yield:

: 1246640-02-7
C₉H₁₁N₅O*ClH

: 1246639-72-4
4-chlorobenzyl 4-[2-(1H-benzotriazol-5-ylcarbamoyl)ethyl-carbamoyl]piperidine-1-carboxylate

Guidance literature:: Multi-step reaction with 3 steps

1.1: triethylamine; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol / N,N-dimethyl-formamide / 16 h / 20 °C

2.1: hydrogenchloride; isopropyl alcohol / 1 h / 20 °C

3.1: N,N-dimethyl-formamide / 2 h / 20 °C

3.2: 16 h / 20 °C

With hydrogenchloride; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; isopropyl alcohol; In N,N-dimethyl-formamide;

Reference yield:

: 1246640-03-8
C₂₀H₂₈N₆O₄

: 1246639-72-4
4-chlorobenzyl 4-[2-(1H-benzotriazol-5-ylcarbamoyl)ethyl-carbamoyl]piperidine-1-carboxylate

Guidance literature:: Multi-step reaction with 2 steps

1.1: hydrogenchloride; isopropyl alcohol / 1 h / 20 °C

2.1: N,N-dimethyl-formamide / 2 h / 20 °C

2.2: 16 h / 20 °C

With hydrogenchloride; isopropyl alcohol; In N,N-dimethyl-formamide;