N₄,N₇-bis(2-bromobenzyl)-N₄,N₇-dibutyl-2,9-dimethyldec-5-yne-4,7-diamine

Base Information

Chemical Name:N₄,N₇-bis(2-bromobenzyl)-N₄,N₇-dibutyl-2,9-dimethyldec-5-yne-4,7-diamine
CAS No.:1376386-85-4
Molecular Formula:C₃₄H₅₀Br₂N₂
Molecular Weight:646.592
Hs Code.:

N<sub>4</sub>,N<sub>7</sub>-bis(2-bromobenzyl)-N<sub>4</sub>,N<sub>7</sub>-dibutyl-2,9-dimethyldec-5-yne-4,7-diamine

Synonyms:N₄,N₇-bis(2-bromobenzyl)-N₄,N₇-dibutyl-2,9-dimethyldec-5-yne-4,7-diamine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N₄,N₇-bis(2-bromobenzyl)-N₄,N₇-dibutyl-2,9-dimethyldec-5-yne-4,7-diamine

Chemical Property:

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Technology Process of N₄,N₇-bis(2-bromobenzyl)-N₄,N₇-dibutyl-2,9-dimethyldec-5-yne-4,7-diamine

There total 3 articles about N₄,N₇-bis(2-bromobenzyl)-N₄,N₇-dibutyl-2,9-dimethyldec-5-yne-4,7-diamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 60509-38-8
N-(2-bromobenzyl)butan-1-amine

: 590-86-3
isovaleraldehyde

: 471-25-0
Propiolic acid

: 1376386-85-4
N₄,N₇-bis(2-bromobenzyl)-N₄,N₇-dibutyl-2,9-dimethyldec-5-yne-4,7-diamine

Guidance literature:: With copper(l) iodide; In toluene; at 100 ℃; for 0.5h; Microwave irradiation;
DOI:10.1021/jo300562j

Reference yield:

: 257628-68-5
N-(2-bromobenzylidene)butan-1-amine

: 1376386-85-4
N₄,N₇-bis(2-bromobenzyl)-N₄,N₇-dibutyl-2,9-dimethyldec-5-yne-4,7-diamine

Guidance literature:: Multi-step reaction with 2 steps

1: sodium tetrahydroborate / methanol / 2 h / 20 °C

2: copper(l) iodide / toluene / 0.5 h / 100 °C / Microwave irradiation

With sodium tetrahydroborate; copper(l) iodide; In methanol; toluene;
DOI:10.1021/jo300562j

Reference yield:

: 6630-33-7
ortho-bromobenzaldehyde

: 1376386-85-4
N₄,N₇-bis(2-bromobenzyl)-N₄,N₇-dibutyl-2,9-dimethyldec-5-yne-4,7-diamine

Guidance literature:: Multi-step reaction with 3 steps

1: toluene / 3 h / Reflux

2: sodium tetrahydroborate / methanol / 2 h / 20 °C

3: copper(l) iodide / toluene / 0.5 h / 100 °C / Microwave irradiation

With sodium tetrahydroborate; copper(l) iodide; In methanol; toluene;
DOI:10.1021/jo300562j