9,10-dimethyl-14-phenyl-9,10-dihydro-9,10-[1,2]epi[1,2,4]triazolo-anthracene-13,15-dione

Base Information

• Chemical Name: 9,10-dimethyl-14-phenyl-9,10-dihydro-9,10-[1,2]epi[1,2,4]triazolo-anthracene-13,15-dione
• CAS No.: 13715-59-8
• Molecular Formula: C₂₄H₁₉N₃O₂
• Molecular Weight: 381.434
• Mol file: 13715-59-8.mol

Synonyms:9,10-dimethyl-14-phenyl-9,10-dihydro-9,10-[1,2]epi[1,2,4]triazolo-anthracene-13,15-dione

Chemical Property of 9,10-dimethyl-14-phenyl-9,10-dihydro-9,10-[1,2]epi[1,2,4]triazolo-anthracene-13,15-dione

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 9,10-dimethyl-14-phenyl-9,10-dihydro-9,10-[1,2]epi[1,2,4]triazolo-anthracene-13,15-dione

There total 14 articles about 9,10-dimethyl-14-phenyl-9,10-dihydro-9,10-[1,2]epi[1,2,4]triazolo-anthracene-13,15-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C34H23N3O2 (1330068-44-4) → 9,10-dimethyl-14-phenyl-9,10-dihydro-9,10-[1,2]epi[1,2,4]triazolo-anthracene-13,15-dione (13715-59-8)

Guidance literature:

Multi-step reaction with 2 steps

1: chloroform-d1 / 50 °C / Darkness

2: chloroform-d1 / 25 °C / Darkness

In chloroform-d1; 1: retro-Diels-Alder Reaction / 2: Diels-Alder reaction;

DOI:10.1002/asia.201100244

Reference yield:

9,10-dimethylanthracene (781-43-1) + C34H23N3O2 (1330068-44-4) → 9,10-dimethyl-14-phenyl-9,10-dihydro-9,10-[1,2]epi[1,2,4]triazolo-anthracene-13,15-dione (13715-59-8)

Guidance literature:

In chloroform-d1; at 25 ℃; Darkness;

DOI:10.1002/asia.201100244

Reference yield:

9,10-dimethylanthracene (781-43-1) + 9,10-(4’-phenyl)urazolo-9,10-dihydroanthracene (10316-56-0) → 9,10-dimethyl-14-phenyl-9,10-dihydro-9,10-[1,2]epi[1,2,4]triazolo-anthracene-13,15-dione (13715-59-8)

Guidance literature:

In chloroform-d1; at 25 ℃; Darkness;

DOI:10.1002/asia.201100244

upstream raw materials:

C₂₃H₁₇N₃O₂

C₃₄H₂₃N₃O₂

9,10-dimethylanthracene

C₂₂H₁₃Cl₂N₃O₂

Downstream raw materials:

9,10-(4’-phenyl)urazolo-9,10-dihydroanthracene

C₃₄H₂₃N₃O₂

C₂₃H₁₇N₃O₂

C₂₂H₁₃Cl₂N₃O₂