Carbonic acid allyl ester 2-allyloxycarbonyloxy-3-[(2R,3R,4R,5R)-2-(4-benzoylamino-2-oxo-2H-pyrimidin-1-yl)-4-hydroxy-5-hydroxymethyl-tetrahydro-furan-3-yloxy]-propyl ester

Base Information

Chemical Name:Carbonic acid allyl ester 2-allyloxycarbonyloxy-3-[(2R,3R,4R,5R)-2-(4-benzoylamino-2-oxo-2H-pyrimidin-1-yl)-4-hydroxy-5-hydroxymethyl-tetrahydro-furan-3-yloxy]-propyl ester
CAS No.:853245-50-8
Molecular Formula:C₂₇H₃₁N₃O₁₂
Molecular Weight:589.556
Hs Code.:

Carbonic acid allyl ester 2-allyloxycarbonyloxy-3-[(2R,3R,4R,5R)-2-(4-benzoylamino-2-oxo-2H-pyrimidin-1-yl)-4-hydroxy-5-hydroxymethyl-tetrahydro-furan-3-yloxy]-propyl ester

Synonyms:Carbonic acid allyl ester 2-allyloxycarbonyloxy-3-[(2R,3R,4R,5R)-2-(4-benzoylamino-2-oxo-2H-pyrimidin-1-yl)-4-hydroxy-5-hydroxymethyl-tetrahydro-furan-3-yloxy]-propyl ester

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Chemical Property of Carbonic acid allyl ester 2-allyloxycarbonyloxy-3-[(2R,3R,4R,5R)-2-(4-benzoylamino-2-oxo-2H-pyrimidin-1-yl)-4-hydroxy-5-hydroxymethyl-tetrahydro-furan-3-yloxy]-propyl ester

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Technology Process of Carbonic acid allyl ester 2-allyloxycarbonyloxy-3-[(2R,3R,4R,5R)-2-(4-benzoylamino-2-oxo-2H-pyrimidin-1-yl)-4-hydroxy-5-hydroxymethyl-tetrahydro-furan-3-yloxy]-propyl ester

There total 3 articles about Carbonic acid allyl ester 2-allyloxycarbonyloxy-3-[(2R,3R,4R,5R)-2-(4-benzoylamino-2-oxo-2H-pyrimidin-1-yl)-4-hydroxy-5-hydroxymethyl-tetrahydro-furan-3-yloxy]-propyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 853245-48-4
Carbonic acid allyl ester 2-allyloxycarbonyloxy-3-[(2R,3R,3aR,9aR)-2-(4-benzoylamino-2-oxo-2H-pyrimidin-1-yl)-5,5,7,7-tetraisopropyl-tetrahydro-1,4,6,8-tetraoxa-5,7-disila-cyclopentacycloocten-3-yloxy]-propyl ester

: 853245-50-8
Carbonic acid allyl ester 2-allyloxycarbonyloxy-3-[(2R,3R,4R,5R)-2-(4-benzoylamino-2-oxo-2H-pyrimidin-1-yl)-4-hydroxy-5-hydroxymethyl-tetrahydro-furan-3-yloxy]-propyl ester

Guidance literature:: With tetrabutyl ammonium fluoride; In tetrahydrofuran; for 0.166667h;
DOI:10.1016/j.tetlet.2005.03.056

Reference yield:

: 176747-26-5
N-{1-[(2R,3R,3aR,9aR)-3-(2,3-Dihydroxy-propoxy)-5,5,7,7-tetraisopropyl-tetrahydro-1,4,6,8-tetraoxa-5,7-disila-cyclopentacycloocten-2-yl]-2-oxo-1,2-dihydro-pyrimidin-4-yl}-benzamide

: 853245-50-8
Carbonic acid allyl ester 2-allyloxycarbonyloxy-3-[(2R,3R,4R,5R)-2-(4-benzoylamino-2-oxo-2H-pyrimidin-1-yl)-4-hydroxy-5-hydroxymethyl-tetrahydro-furan-3-yloxy]-propyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 82 percent / Et₃N / CH₂Cl₂ / 1 h / 4 °C

2: 91 percent / TBAF / tetrahydrofuran / 0.17 h

With tetrabutyl ammonium fluoride; triethylamine; In tetrahydrofuran; dichloromethane;
DOI:10.1016/j.tetlet.2005.03.056

Reference yield:

: N-[1-((2R,3R,3aR,9aR)-3-Allyloxy-5,5,7,7-tetraisopropyl-tetrahydro-1,4,6,8-tetraoxa-5,7-disila-cyclopentacycloocten-2-yl)-2-oxo-1,2-dihydro-pyrimidin-4-yl]-benzamide

: 853245-50-8
Carbonic acid allyl ester 2-allyloxycarbonyloxy-3-[(2R,3R,4R,5R)-2-(4-benzoylamino-2-oxo-2H-pyrimidin-1-yl)-4-hydroxy-5-hydroxymethyl-tetrahydro-furan-3-yloxy]-propyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 92 percent / OsO₄; N-methylmorpholine N-oxide / tetrahydrofuran; H₂O / 1 h

2: 82 percent / Et₃N / CH₂Cl₂ / 1 h / 4 °C

3: 91 percent / TBAF / tetrahydrofuran / 0.17 h

With osmium(VIII) oxide; tetrabutyl ammonium fluoride; 4-methylmorpholine N-oxide; triethylamine; In tetrahydrofuran; dichloromethane; water;
DOI:10.1016/j.tetlet.2005.03.056