10-(p-methoxyphenyl)-4-oxo-3-phenyl-1,2,3,4-tetrahydro-2-thioxocyclopenta-[5',6']pyrido[3',2':4,5]thieno[3,2-d]pyrimidine

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Chemical Name:10-(p-methoxyphenyl)-4-oxo-3-phenyl-1,2,3,4-tetrahydro-2-thioxocyclopenta-[5',6']pyrido[3',2':4,5]thieno[3,2-d]pyrimidine
CAS No.:302554-54-7
Molecular Formula:C₂₅H₁₉N₃O₂S₂
Molecular Weight:457.577
Hs Code.:

Synonyms:10-(p-methoxyphenyl)-4-oxo-3-phenyl-1,2,3,4-tetrahydro-2-thioxocyclopenta-[5',6']pyrido[3',2':4,5]thieno[3,2-d]pyrimidine

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Chemical Property of 10-(p-methoxyphenyl)-4-oxo-3-phenyl-1,2,3,4-tetrahydro-2-thioxocyclopenta-[5',6']pyrido[3',2':4,5]thieno[3,2-d]pyrimidine

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Technology Process of 10-(p-methoxyphenyl)-4-oxo-3-phenyl-1,2,3,4-tetrahydro-2-thioxocyclopenta-[5',6']pyrido[3',2':4,5]thieno[3,2-d]pyrimidine

There total 10 articles about 10-(p-methoxyphenyl)-4-oxo-3-phenyl-1,2,3,4-tetrahydro-2-thioxocyclopenta-[5',6']pyrido[3',2':4,5]thieno[3,2-d]pyrimidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 103-72-0
phenyl isothiocyanate

: 302554-36-5
3-amino-4-(4-methoxy-phenyl)-6,7-dihydro-5H-1-thia-8-aza-s-indacene-2-carboxylic acid amide

: 302554-54-7
10-(p-methoxyphenyl)-4-oxo-3-phenyl-1,2,3,4-tetrahydro-2-thioxocyclopenta-[5',6']pyrido[3',2':4,5]thieno[3,2-d]pyrimidine

Guidance literature:: In acetic acid; for 8h; Heating;

Reference yield: 67.0%

: 75-15-0,12122-00-8
carbon disulfide

: 345912-40-5
3-amino-4-(4-methoxy-phenyl)-6,7-dihydro-5H-1-thia-8-aza-s-indacene-2-carboxylic acid phenylamide

: 302554-54-7
10-(p-methoxyphenyl)-4-oxo-3-phenyl-1,2,3,4-tetrahydro-2-thioxocyclopenta-[5',6']pyrido[3',2':4,5]thieno[3,2-d]pyrimidine

Guidance literature:: In pyridine; for 8h; Heating;
DOI:10.1080/10426500008076538

Reference yield:

: 120517-49-9
4-(4-methoxyphenyl)-2-sulfanylidene-1H,2H,5H,6H,7H-cyclopenta[b]pyridine-3-carbonitrile

: 302554-54-7
10-(p-methoxyphenyl)-4-oxo-3-phenyl-1,2,3,4-tetrahydro-2-thioxocyclopenta-[5',6']pyrido[3',2':4,5]thieno[3,2-d]pyrimidine

Guidance literature:: Multi-step reaction with 3 steps

1: 80 percent / AcONa*3H₂O / ethanol / 2 h / Heating

2: 93 percent / EtONa / ethanol / 0.08 h / Heating

3: 67 percent / pyridine / 8 h / Heating

With sodium ethanolate; sodium acetate; In pyridine; ethanol; 2: Thorpe-Ziegler cyclization;
DOI:10.1080/10426500008076538